(2,9-dimethyl-4,7-diphenyl-1,10-phenantroline)NiBr2

Base Information

• Chemical Name: (2,9-dimethyl-4,7-diphenyl-1,10-phenantroline)NiBr2
• CAS No.: 326822-02-0
• Molecular Formula: C₂₆H₂₀Br₂N₂Ni
• Molecular Weight: 578.956

Synonyms:

Chemical Property of (2,9-dimethyl-4,7-diphenyl-1,10-phenantroline)NiBr2

Chemical Property:

• Melting Point: >300 °C

Purity/Quality:

98%,99%, ^*data from raw suppliers

(Bathocuproine)NiBr2 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: Catalyst for C-alkylation of nitroalkanes with unactivated alkyl iodides

Technology Process of (2,9-dimethyl-4,7-diphenyl-1,10-phenantroline)NiBr2

There total 2 articles about (2,9-dimethyl-4,7-diphenyl-1,10-phenantroline)NiBr2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

nickel(II) bromide diethylene glycol dimethyl ether + Bathocuproine (4733-39-5) → (2,9-dimethyl-4,7-diphenyl-1,10-phenantroline)NiBr2 (326822-02-0)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 46h; Inert atmosphere; Sealed tube;

DOI:10.1021/jacs.7b04312

Reference yield: 12.3%

nickel(II) dibromide trihydrate + Bathocuproine (4733-39-5) → (2,9-dimethyl-4,7-diphenyl-1,10-phenantroline)NiBr2 (326822-02-0)

Guidance literature:

In methanol; ligand and NiBr2*3H2O were suspended in MeOH, stirred for 30 h at room temp. under N2; filtered, washed by refluxing in toluene, filtered, dried under vac., crystd. from CH2Cl2; elem. anal.;

DOI:10.1016/S0022-328X(00)00618-5

upstream raw materials:

Bathocuproine

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