benzyl 2-{2'-(N,N-dimethylamino)ethyl}phenyl selenide

Base Information

Chemical Name:benzyl 2-{2'-(N,N-dimethylamino)ethyl}phenyl selenide
CAS No.:1011722-61-4
Molecular Formula:C₁₇H₂₁NSe
Molecular Weight:318.32
Hs Code.:

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Chemical Property of benzyl 2-{2'-(N,N-dimethylamino)ethyl}phenyl selenide

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Technology Process of benzyl 2-{2'-(N,N-dimethylamino)ethyl}phenyl selenide

There total 1 articles about benzyl 2-{2'-(N,N-dimethylamino)ethyl}phenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 1482-82-2
dibenzyl diselenide

: 2410-47-1
2-{2'-(N,N-dimethylamino)ethyl}bromobenzene

: 1011722-61-4
benzyl 2-{2'-(N,N-dimethylamino)ethyl}phenyl selenide

Guidance literature:: With magnesium; In tetrahydrofuran; at 0 - 20 ℃; for 16h;
DOI:10.1002/hc.20299

Reference yield: 24.0%

: 1011722-61-4
benzyl 2-{2'-(N,N-dimethylamino)ethyl}phenyl selenide

: 1011722-62-5
benzyl 2-{2'-(N,N-dimethylamino)ethyl}phenyl selenoxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 5h;
DOI:10.1002/hc.20299

Reference yield:

: 1011722-61-4
benzyl 2-{2'-(N,N-dimethylamino)ethyl}phenyl selenide

: 1011722-72-7
(S)-(-)-benzyl 2-{2'-(N,N-dimethylamino)ethyl}phenyl selenoxide

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 5 h / 0 - 20 °C

2: amylose carbamate derivative/silica gel(Daicel Chiralpak AS) / hexane; ethanol

With 3-chloro-benzenecarboperoxoic acid; In ethanol; hexane; dichloromethane;
DOI:10.1002/hc.20299