benzyl N,N-diethyl-(S)-glutaminate hydrochloridee

Base Information

Chemical Name:benzyl N,N-diethyl-(S)-glutaminate hydrochloridee
CAS No.:77529-80-7
Molecular Formula:C₁₆H₂₄N₂O₃*ClH
Molecular Weight:328.839
Hs Code.:

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Chemical Property of benzyl N,N-diethyl-(S)-glutaminate hydrochloridee

Chemical Property:

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Technology Process of benzyl N,N-diethyl-(S)-glutaminate hydrochloridee

There total 2 articles about benzyl N,N-diethyl-(S)-glutaminate hydrochloridee which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77529-79-4
benzyl N²-(tert-butoxycarbonyl)-N,N-diethyl-(S)-glutaminate

: 77529-80-7
benzyl N,N-diethyl-(S)-glutaminate hydrochloridee

Guidance literature:: With hydrogenchloride; In diethyl ether; for 0.5h;
DOI:10.1021/jm00138a014

Reference yield:

: 30924-93-7
Boc-Glu-OBn

: 77529-80-7
benzyl N,N-diethyl-(S)-glutaminate hydrochloridee

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1-hydroxybenzotriazole, dicyclohexylcarbodiimide (DCC) / 1.) THF, 0 deg C, 1 h, 2.) THF, RT, 8 h

2: HCl (gas) / diethyl ether / 0.5 h

With hydrogenchloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In diethyl ether;
DOI:10.1021/jm00138a014

Reference yield:

: 77529-80-7
benzyl N,N-diethyl-(S)-glutaminate hydrochloridee

: 77529-95-4
(S)-7-chloro-4-<<1'-(hydroxymethyl)-4'-(diethylamino)butyl>amino>quinoline

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / ethanol / 1 h / 2068.6 Torr / Ambient temperature

2: 75 percent / LiAlH₄ / tetrahydrofuran / Heating

3: 56 percent / phenol / 19 h / 125 °C

With lithium aluminium tetrahydride; hydrogen; phenol; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00138a014