(2R,3R,4S,5S,6R)-2-((1S,2S,3R,4R,6S)-4-Amino-2,3-dihydroxy-6-hydroxymethyl-cyclohexyloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol; hydrochloride

Base Information

Chemical Name:(2R,3R,4S,5S,6R)-2-((1S,2S,3R,4R,6S)-4-Amino-2,3-dihydroxy-6-hydroxymethyl-cyclohexyloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol; hydrochloride
CAS No.:73651-18-0
Molecular Formula:C₁₃H₂₅NO₉*ClH
Molecular Weight:375.804
Hs Code.:

(2R,3R,4S,5S,6R)-2-((1S,2S,3R,4R,6S)-4-Amino-2,3-dihydroxy-6-hydroxymethyl-cyclohexyloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol; hydrochloride

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Chemical Property of (2R,3R,4S,5S,6R)-2-((1S,2S,3R,4R,6S)-4-Amino-2,3-dihydroxy-6-hydroxymethyl-cyclohexyloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol; hydrochloride

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Technology Process of (2R,3R,4S,5S,6R)-2-((1S,2S,3R,4R,6S)-4-Amino-2,3-dihydroxy-6-hydroxymethyl-cyclohexyloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol; hydrochloride

There total 8 articles about (2R,3R,4S,5S,6R)-2-((1S,2S,3R,4R,6S)-4-Amino-2,3-dihydroxy-6-hydroxymethyl-cyclohexyloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2R,3R,4S,5S,6R)-2-((1R,2R,3S,4S,6R)-4-Azido-2,3-dihydroxy-6-hydroxymethyl-cyclohexyloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

: 73651-18-0,73651-20-4
(2R,3R,4S,5S,6R)-2-((1R,2R,3S,4S,6R)-4-Amino-2,3-dihydroxy-6-hydroxymethyl-cyclohexyloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol; hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; Yield given;
DOI:10.1246/cl.1980.139

Reference yield:

: (2R,3R,4S,5S,6R)-2-((1S,2S,3R,4R,6S)-4-Azido-2,3-dihydroxy-6-hydroxymethyl-cyclohexyloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

: 73651-18-0,73651-20-4
(2R,3R,4S,5S,6R)-2-((1S,2S,3R,4R,6S)-4-Amino-2,3-dihydroxy-6-hydroxymethyl-cyclohexyloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol; hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; Yield given;
DOI:10.1246/cl.1980.139

Reference yield:

: 73411-02-6
DL-2,3-O-isopropylidene-(1,3/2,4,6)-6-benzoyloxymethyl-4-bromo-1,2,3-cyclohexanetriol

: 73651-18-0,73651-20-4
(2R,3R,4S,5S,6R)-2-((1R,2R,3S,4S,6R)-4-Amino-2,3-dihydroxy-6-hydroxymethyl-cyclohexyloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / sodium azide / dimethylsulfoxide / 18 h / 120 °C

2: 1.) mercuric(II) cyanide, calcium sulfate; 2.) Amberlite IR-120B (H⁽¹⁺⁾) / 1.) benzene, 70 deg C, 50 h; 2.) ethanol, r.t., overnight

3: sodium methoxide / methanol

4: hydrogen, HCl / 5percent palladium on carbon / ethanol

With hydrogenchloride; calcium sulfate; sodium azide; Amberlite IR-120B (H⁽¹⁺⁾); hydrogen; sodium methylate; mercury(II) cyanide; palladium on activated charcoal; In methanol; ethanol; dimethyl sulfoxide;
DOI:10.1246/cl.1980.139