[zinc(phenyldithiocarboxylic acid-H)2(N,N,N',N'-tetramethylethylenediamine)]

Base Information

• Chemical Name: [zinc(phenyldithiocarboxylic acid-H)2(N,N,N',N'-tetramethylethylenediamine)]
• CAS No.: 1010688-57-9
• Molecular Formula: C₂₀H₂₆N₂S₄Zn
• Molecular Weight: 488.094
• Mol file: 1010688-57-9.mol

Synonyms:

Chemical Property of [zinc(phenyldithiocarboxylic acid-H)2(N,N,N',N'-tetramethylethylenediamine)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [zinc(phenyldithiocarboxylic acid-H)2(N,N,N',N'-tetramethylethylenediamine)]

There total 2 articles about [zinc(phenyldithiocarboxylic acid-H)2(N,N,N',N'-tetramethylethylenediamine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(tetramethylethylenediamine)Zn(OAc)2 + dithiobenzoic acid (121-68-6) → [zinc(phenyldithiocarboxylic acid-H)2(N,N,N',N'-tetramethylethylenediamine)] (1010688-57-9)

Guidance literature:

In benzene; byproducts: CH3COOH; solid Zn complex (1.97 mmol) added to soln. of phenyldithiocarboxylic acid (3.92 mmol) (vigorous stirring); stirred (2 h) under N2; solvent evapd. (vac.); recrystd. from CH2Cl2-toluene; elem. anal.;

DOI:10.1002/ejic.200601059

Reference yield:

N,N,N,N,-tetramethylethylenediamine (110-18-9) → [zinc(phenyldithiocarboxylic acid-H)2(N,N,N',N'-tetramethylethylenediamine)] (1010688-57-9)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane

2: benzene

In dichloromethane; benzene;

DOI:10.1002/ejic.200601059

upstream raw materials:

dithiobenzoic acid

N,N,N,N,-tetramethylethylenediamine