tricarbonyl(η4-2,5-diphenylthiophene dioxide)iron

Base Information

Chemical Name:tricarbonyl(η4-2,5-diphenylthiophene dioxide)iron
CAS No.:132080-68-3
Molecular Formula:C₁₉H₁₂FeO₅S
Molecular Weight:408.214
Hs Code.:

Synonyms:

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Chemical Property of tricarbonyl(η4-2,5-diphenylthiophene dioxide)iron

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Technology Process of tricarbonyl(η4-2,5-diphenylthiophene dioxide)iron

There total 2 articles about tricarbonyl(η4-2,5-diphenylthiophene dioxide)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 51092-02-5
2,5-bis(phenyl)-thiophene-1,1-dioxide

: 132080-68-3
tricarbonyl(η4-2,5-diphenylthiophene dioxide)iron

Guidance literature:: In benzene; byproducts: 2,5-diphenylthiophene; Irradiation (UV/VIS); under inert gas; to a solution of the 2,5-DPTDO was added Fe(CO)5; was irradiated for 6 h at room temperature; CH2Cl2 also may be used as solvent; filtration; evapn. to dryness; chromy. (toluene); elution with toluene, ethyl acetate; recrystn. from pentane/CH2Cl2; elem. anal.;
DOI:10.1016/0022-328X(90)80095-H

Reference yield: 45.0%

: 15321-51-4
diiron nonacarbonyl

: 51092-02-5
2,5-bis(phenyl)-thiophene-1,1-dioxide

: 132080-68-3
tricarbonyl(η4-2,5-diphenylthiophene dioxide)iron

Guidance literature:: In tetrahydrofuran; byproducts: Fe3(CO)12; under inert gas; a solution of 2,5-DPTDO and Fe2(CO)9 was stirred for 4 h under exclusion of light; filtration; evapn. to dryness; chromy. with toluene; elution with toluene and then with ethyl acetate; elem. anal.;
DOI:10.1016/0022-328X(90)80095-H

Reference yield: 40.0%

: 132080-68-3
tricarbonyl(η4-2,5-diphenylthiophene dioxide)iron

: 132080-91-2
Fe(CO)2(P(C₆H₅)3)(C₄H₂(C₆H₅)2SO₂)

Guidance literature:: With PPh₃; In toluene; Irradiation (UV/VIS); under inert gas; PPh3 and the Fe-complex were irradiated for 6 h; filtration; dried in vacuo;;
DOI:10.1016/0022-328X(90)80095-H