(1,1-diphenyl-1-hydroxy-2-propanone)tricarbonylchromium

Base Information

Chemical Name:(1,1-diphenyl-1-hydroxy-2-propanone)tricarbonylchromium
CAS No.:104764-95-6
Molecular Formula:C₁₈H₁₄CrO₅
Molecular Weight:362.302
Hs Code.:

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Chemical Property of (1,1-diphenyl-1-hydroxy-2-propanone)tricarbonylchromium

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Technology Process of (1,1-diphenyl-1-hydroxy-2-propanone)tricarbonylchromium

There total 1 articles about (1,1-diphenyl-1-hydroxy-2-propanone)tricarbonylchromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.5%

: 12147-92-1
(benzophenone)tricarbonylchromium(0)

: 104764-95-6
(1,1-diphenyl-1-hydroxy-2-propanone)tricarbonylchromium

: 104764-94-5
(benzhydryl acetate)tricarbonylchromium

: 104764-93-4
(1,1-diphenyl-1-acetoxy-2-propanone)tricarbonylchromium

Guidance literature:: With acetic anhydride; In N,N-dimethyl-formamide; Electrolysis; under Ar; electroredn. of Cr-complex in the presence of 12.5 equiv. in DMF/(CH3CO)2O (potential changed from -1.31 to -1.50 V, H-type cell, Hg and Pt electrodes, 0.1M Bu4NPF6 or Bu4NBF4), halted when the Faradaic current became negligible (n=1.82); catholyte dild. with water, dropwise addn. 1M NaOH/H2O until pH8, extd. (Et2O), Et2O-soln. dried, evapn., column chromy. (1:1 Et2O:hexane), traces of starting Cr-complex also present, elem. anal.;
DOI:10.1016/0022-328X(86)84038-4