{Mo((C₆H₅)2(C₆H₃S))2(CO)}

Base Information

Chemical Name:{Mo((C₆H₅)2(C₆H₃S))2(CO)}
CAS No.:97286-53-8
Molecular Formula:C₃₇H₂₆MoOS₂
Molecular Weight:646.685
Hs Code.:

{Mo((C<sub>6</sub>H<sub>5</sub>)2(C<sub>6</sub>H<sub>3</sub>S))2(CO)}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {Mo((C₆H₅)2(C₆H₃S))2(CO)}

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Technology Process of {Mo((C₆H₅)2(C₆H₃S))2(CO)}

There total 2 articles about {Mo((C₆H₅)2(C₆H₃S))2(CO)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.3%

: 22172-30-1
dibromotetracarbonylmolybdenum(II)

: 97222-10-1
sodium-2,6-diphenylthiophenolate

: 97286-53-8
{Mo((C₆H₅)2(C₆H₃S))2(CO)}

Guidance literature:: In 1,2-dimethoxyethane; dropwise addn. of Na salt soln. to Mo complex soln. under N2; stirring, 12h; filtration; evapn. to dryness; titrating with warm hexane, 5 min; pptn.; elem. anal.;

Reference yield: 73.3%

: 15712-13-7
dichlorotetracarbonylmolybdenum

: 97222-10-1
sodium-2,6-diphenylthiophenolate

: 97286-53-8
{Mo((C₆H₅)2(C₆H₃S))2(CO)}

Guidance literature:: In 1,2-dimethoxyethane; stirring for 12 h;; filtration through Celite, filtrate evapd. to dryness, the resulting green-yellow oil was triturated with warm hexane for 5 min, elem. anal.;;
DOI:10.1039/DT9910000385

Reference yield: 70.0%

: 66-71-7
1,10-Phenanthroline

: 97286-53-8
{Mo((C₆H₅)2(C₆H₃S))2(CO)}

: 134026-46-3
{Mo(dpt)2(CO)2(phen)}

Guidance literature:: In 1,2-dimethoxyethane; react. time 3 h;; evapn. to dryness, residue chromd. on neutral alumina column using CH2Cl2 as solvent, dark purple band eluted, collected, solvent removed under reduced pressure yielding oil; triturated with diethyl-ether, dried in vac., elem. anal.;;
DOI:10.1039/DT9910000385