Technology Process of C30H24ClF3N4O5
There total 6 articles about C30H24ClF3N4O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: caesium carbonate / N,N-dimethyl-formamide / 15 h / 20 °C
2: 1-methyl-pyrrolidin-2-one / 2.5 h / 140 °C
With
caesium carbonate;
In
1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide;
DOI:10.1021/jm2008634
- Guidance literature:
-
Multi-step reaction with 2 steps
1: platinum on carbon; hydrogen / ethyl acetate / 2 h / 20 °C
2: 1-methyl-pyrrolidin-2-one / 2.5 h / 140 °C
With
platinum on carbon; hydrogen;
In
1-methyl-pyrrolidin-2-one; ethyl acetate;
DOI:10.1021/jm2008634
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C
2: platinum on carbon; hydrogen / ethyl acetate / 2 h / 20 °C
3: 1-methyl-pyrrolidin-2-one / 2.5 h / 140 °C
With
platinum on carbon; hydrogen; potassium carbonate;
In
1-methyl-pyrrolidin-2-one; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm2008634