C₁₄H₁₉F₃NO₁₄P₃

Base Information

Chemical Name:C₁₄H₁₉F₃NO₁₄P₃
CAS No.:1364927-49-0
Molecular Formula:C₁₄H₁₉F₃NO₁₄P₃
Molecular Weight:575.22
Hs Code.:

C<sub>14</sub>H<sub>19</sub>F<sub>3</sub>NO<sub>14</sub>P<sub>3</sub>

Synonyms:

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Chemical Property of C₁₄H₁₉F₃NO₁₄P₃

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Technology Process of C₁₄H₁₉F₃NO₁₄P₃

There total 10 articles about C₁₄H₁₉F₃NO₁₄P₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1364927-40-1
C₁₄H₁₆F₃NO₅

: 1364927-49-0
C₁₄H₁₉F₃NO₁₄P₃

Guidance literature:: C₁₄H₁₆F₃NO₅; With trimethyl phosphite; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate; at -15 - -10 ℃; Inert atmosphere;

With tributyl-amine; tri-n-butylamine pyrophosphate; In N,N-dimethyl-formamide; at -10 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/chem.201102066

Reference yield:

: C₂₁H₂₅NO₆

: 1364927-49-0
C₁₄H₁₉F₃NO₁₄P₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / 2.15 h / 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 1 h / 20 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 0.33 h / 10 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

5.1: trimethyl phosphite; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate / -15 - -10 °C / Inert atmosphere

5.2: 0.5 h / -10 °C / Inert atmosphere

With pyridine; trimethyl phosphite; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; triethylamine; trichlorophosphate; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1002/chem.201102066

Reference yield:

: 1241725-14-3
C₁₇H₃₆O₃Si₂

: 1364927-49-0
C₁₄H₁₉F₃NO₁₄P₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: tributyl-amine; triphenyl-arsane; palladium diacetate / N,N-dimethyl-formamide / 15 h / 20 - 70 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

3.1: sodium triacetoxyborohydride; acetic acid / acetonitrile / 1 h / 0 °C / Inert atmosphere

4.1: pyridine / 2.15 h / 20 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 1 h / 20 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 0.33 h / 10 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

8.1: trimethyl phosphite; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate / -15 - -10 °C / Inert atmosphere

8.2: 0.5 h / -10 °C / Inert atmosphere

With pyridine; trimethyl phosphite; tributyl-amine; triphenyl-arsane; palladium 10% on activated carbon; sodium triacetoxyborohydride; tetrabutyl ammonium fluoride; hydrogen; palladium diacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; acetic acid; triethylamine; trichlorophosphate; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 1.1: Heck reaction;
DOI:10.1002/chem.201102066