4-Nitro-benzoyloxythioameisensaeure-S-, 4-Nitro-benzoesaeure--anhydrid

Base Information

• Chemical Name: 4-Nitro-benzoyloxythioameisensaeure-S-, 4-Nitro-benzoesaeure--anhydrid
• CAS No.: 16118-27-7
• Molecular Formula: C₁₂H₁₃NO₅S
• Molecular Weight: 283.305

Synonyms:

Chemical Property of 4-Nitro-benzoyloxythioameisensaeure-S-, 4-Nitro-benzoesaeure--anhydrid

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 4-Nitro-benzoyloxythioameisensaeure-S-, 4-Nitro-benzoesaeure--anhydrid

There total 2 articles about 4-Nitro-benzoyloxythioameisensaeure-S-, 4-Nitro-benzoesaeure--anhydrid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

t-butyl chlorothioformate (13889-95-7) + 4-nitro-benzoic acid (62-23-7) → 4-Nitro-benzoyloxythioameisensaeure-S-, 4-Nitro-benzoesaeure--anhydrid (16118-27-7)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; In tetrahydrofuran;

DOI:10.1021/jo01269a039

Reference yield:

→ 4-Nitro-benzoyloxythioameisensaeure-S-, 4-Nitro-benzoesaeure--anhydrid (16118-27-7)

Guidance literature:

4-Nitro-benzoesaeure, Thiokohlensaeurechlorid-S-B in Ae. bei -5grad, Triaethylamin;

DOI:10.1021/jo01031a521

Reference yield:

4-Nitro-benzoyloxythioameisensaeure-S-, 4-Nitro-benzoesaeure--anhydrid (16118-27-7) + N-methylaniline (100-61-8) → N-methyl-N-phenyl-4-nitrobenzamide (961-61-5)

Guidance literature:

In diethyl ether;

DOI:10.1021/jo01269a039

upstream raw materials:

t-butyl chlorothioformate

4-nitro-benzoic acid

Downstream raw materials:

4-Nitro-thiobenzoesaeure-S-

N-methyl-N-phenyl-4-nitrobenzamide

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