Technology Process of C18H15NO4S
There total 6 articles about C18H15NO4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Au(OAc)3 / 1,2-dichloro-ethane / 20 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / 20 °C / Inert atmosphere
3: hydrogenchloride / water; ethyl acetate / Inert atmosphere
4: polystyrene supported 4-dimethylaminopyridine / dichloromethane / Inert atmosphere
With
hydrogenchloride; Au(OAc)3; tetrabutyl ammonium fluoride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1021/co300002x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / water; ethyl acetate / Inert atmosphere
2: polystyrene supported 4-dimethylaminopyridine / dichloromethane / Inert atmosphere
With
hydrogenchloride;
In
dichloromethane; water; ethyl acetate;
DOI:10.1021/co300002x
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / 20 °C / Inert atmosphere
2: hydrogenchloride / water; ethyl acetate / Inert atmosphere
3: polystyrene supported 4-dimethylaminopyridine / dichloromethane / Inert atmosphere
With
hydrogenchloride; tetrabutyl ammonium fluoride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dichloromethane; water; ethyl acetate;
DOI:10.1021/co300002x