C₂₂H₂₃ClO

Base Information

Chemical Name:C₂₂H₂₃ClO
CAS No.:1393376-24-3
Molecular Formula:C₂₂H₂₃ClO
Molecular Weight:338.877
Hs Code.:

Synonyms:

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Chemical Property of C₂₂H₂₃ClO

Chemical Property:

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Technology Process of C₂₂H₂₃ClO

There total 6 articles about C₂₂H₂₃ClO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1393376-38-9
C₂₂H₂₁ClO

: 1393376-24-3
C₂₂H₂₃ClO

: C₂₂H₂₃ClO

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201202125

Reference yield:

: 1393376-60-7
C₁₈H₁₈O₃S

: 1393376-24-3
C₂₂H₂₃ClO

: C₂₂H₂₃ClO

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / 1-methyl-pyrrolidin-2-one; paraffin oil / 0.33 h / 0 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 48 h / 20 °C / Inert atmosphere

3.1: (R)-(+)-2,2'-bis[bis(3,5-dimethylphenyl)phosphino]-1,1'-binaphthyl; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / 1,2-dichloro-ethane / 90 h / 80 °C / Inert atmosphere

4.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1 h / 20 °C / Inert atmosphere

With (R)-(+)-2,2'-bis[bis(3,5-dimethylphenyl)phosphino]-1,1'-binaphthyl; sodium tetrahydroborate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; sodium hydride; triethylamine; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; 1,2-dichloro-ethane; paraffin oil;
DOI:10.1002/anie.201202125

Reference yield:

: 1393376-59-4
C₁₁H₁₂O

: 1393376-24-3
C₂₂H₂₃ClO

: C₂₂H₂₃ClO

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / 1-methyl-pyrrolidin-2-one; paraffin oil / 0.33 h / 0 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 48 h / 20 °C / Inert atmosphere

4.1: (R)-(+)-2,2'-bis[bis(3,5-dimethylphenyl)phosphino]-1,1'-binaphthyl; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / 1,2-dichloro-ethane / 90 h / 80 °C / Inert atmosphere

5.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1 h / 20 °C / Inert atmosphere

With (R)-(+)-2,2'-bis[bis(3,5-dimethylphenyl)phosphino]-1,1'-binaphthyl; sodium tetrahydroborate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; sodium hydride; triethylamine; potassium hydroxide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; 1,2-dichloro-ethane; paraffin oil;
DOI:10.1002/anie.201202125