C₁₈H₁₂Br₃ClN₂O₂

Base Information

Chemical Name:C₁₈H₁₂Br₃ClN₂O₂
CAS No.:1422285-78-6
Molecular Formula:C₁₈H₁₂Br₃ClN₂O₂
Molecular Weight:563.47
Hs Code.:

C<sub>18</sub>H<sub>12</sub>Br<sub>3</sub>ClN<sub>2</sub>O<sub>2</sub>

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Chemical Property of C₁₈H₁₂Br₃ClN₂O₂

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Technology Process of C₁₈H₁₂Br₃ClN₂O₂

There total 7 articles about C₁₈H₁₂Br₃ClN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1422285-77-5
C₁₈H₁₃Br₃N₂O₃

: 1422285-78-6
C₁₈H₁₂Br₃ClN₂O₂

Guidance literature:: With trichlorophosphate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.12.033

Reference yield:

: 1422285-76-4
C₁₈H₁₄Br₃NO₅

: 1422285-78-6
C₁₈H₁₂Br₃ClN₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate / ethanol

2: trichlorophosphate / N,N-dimethyl-formamide

With ammonium acetate; trichlorophosphate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.12.033

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 1422285-78-6
C₁₈H₁₂Br₃ClN₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1: bromine / acetic acid / 2 h / 20 °C

2: bromine / chloroform / 2 h / 20 °C

3: chloroform / 18 h / 20 °C

4: hydrogen bromide / methanol / 48 h

5: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 4-methyl-morpholine / N,N-dimethyl-formamide / 2 h / 20 °C

6: ammonium acetate / ethanol

7: trichlorophosphate / N,N-dimethyl-formamide

With 4-methyl-morpholine; ammonium acetate; hydrogen bromide; bromine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; trichlorophosphate; In methanol; ethanol; chloroform; acetic acid; N,N-dimethyl-formamide; 2: |Delepine Amine Synthesis;
DOI:10.1016/j.bmcl.2012.12.033