(S)-(+)-N-methyl-N-1-phenylethylaminodiphenylphosphane

Base Information

Chemical Name:(S)-(+)-N-methyl-N-1-phenylethylaminodiphenylphosphane
CAS No.:76152-62-0
Molecular Formula:C₂₁H₂₂NP
Molecular Weight:319.386
Hs Code.:

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Chemical Property of (S)-(+)-N-methyl-N-1-phenylethylaminodiphenylphosphane

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Technology Process of (S)-(+)-N-methyl-N-1-phenylethylaminodiphenylphosphane

There total 9 articles about (S)-(+)-N-methyl-N-1-phenylethylaminodiphenylphosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: (+)436-CpFe(CO)(COMe)PPh₂NMeCHMePh

: dicarbonyl(cyclopentadienyl)methyliron(II)

: (-)436-CpFe(CO)(COMe)PPh₂NMeCHMePh

: (R)-{(η5-C5H5)Fe(CO)(PPh3)(Ac)}

: 76152-62-0
(S)-(+)-N-methyl-N-1-phenylethylaminodiphenylphosphane

: (S)-{(η5-C5H5)Fe(CO)(PPh3)(Ac)}

Guidance literature:: With triphenylphosphine; In benzene-d6; sealed tube, under exclusion of air, moisture and light, 90°C, 4 h; cooled rapidly to room temp.; chromd. (SiO2) with benzene, then (main products) with ether; epimer sepn. by liq. chromy.; opt. purity after react.: starting material 86%, (+)-react. product 56%;

Reference yield: 15.0%

: (-)436-CpFe(CO)(COMe)PPh₂NMeCHMePh

: dicarbonyl(cyclopentadienyl)methyliron(II)

: (R)-{(η5-C5H5)Fe(CO)(PPh3)(Ac)}

: 76152-62-0
(S)-(+)-N-methyl-N-1-phenylethylaminodiphenylphosphane

: (S)-{(η5-C5H5)Fe(CO)(PPh3)(Ac)}

: (+)436-CpFe(CO)(COMe)PPh₂NMeCHMePh

Guidance literature:: With triphenylphosphine; In benzene; sealed tube, under exclusion of air, moisture and light, 90°C, 42 h; cooled rapidly to room temp.; chromd. (SiO2) with benzene, then (main products) with ether; epimer sepn. by liq. chromy.; opt. purity after react.: starting material 85%, (-)-react. product 60%;

Reference yield: 12.0%

: 931-53-3
Cyclohexyl isocyanide

: (+)436-CpFe(CO)(COMe)PPh₂NMeCHMePh

: dicarbonyl(cyclopentadienyl)methyliron(II)

: (-)436-CpFe(CO)(COMe)PPh₂NMeCHMePh

: 76152-62-0
(S)-(+)-N-methyl-N-1-phenylethylaminodiphenylphosphane

: (C₅H₅)Fe(COCH₃)(CO)(CNC₆H₁₁)

Guidance literature:: In benzene-d6; sealed tube, under exclusion of air, moisture and light, 90°C, 26 h; cooled rapidly to room temp.; chromd. (SiO2) with benzene, then (main products) with ether; epimer sepn. by liq. chromy.; opt. purity starting material 23% after react.;