mer,trans-[Mn(CO)3H(PEtPh₂)2]

Base Information

Chemical Name:mer,trans-[Mn(CO)3H(PEtPh₂)2]
CAS No.:61943-36-0
Molecular Formula:C₃₁H₃₁MnO₃P₂
Molecular Weight:568.471
Hs Code.:

mer,trans-[Mn(CO)3H(PEtPh<sub>2</sub>)2]

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of mer,trans-[Mn(CO)3H(PEtPh₂)2]

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Technology Process of mer,trans-[Mn(CO)3H(PEtPh₂)2]

There total 3 articles about mer,trans-[Mn(CO)3H(PEtPh₂)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 16940-66-2
sodium tetrahydroborate

: 10170-69-1
dimanganese decacarbonyl

: 607-01-2
ethyl-diphenyl-phosphane

: 61943-36-0
mer,trans-[Mn(CO)3H(PEtPh₂)2]

Guidance literature:: With ethanol; In ethanol; large excess of phosphine, refluxing for 10 h; evapn. (reduced pressure), washing (water), recrystn. (Me2CO/EtOH);
DOI:10.1039/DT9760002109

Reference yield: 65.0%

: 10170-69-1
dimanganese decacarbonyl

: 607-01-2
ethyl-diphenyl-phosphane

: 61943-36-0
mer,trans-[Mn(CO)3H(PEtPh₂)2]

Guidance literature:: In propan-1-ol; large excess of phosphine, refluxing for 15 h; cooling (pptn.), recrystn. (Et2O/EtOH); elem. anal.;
DOI:10.1039/DT9760002109

Reference yield:

: 10170-69-1
dimanganese decacarbonyl

: 607-01-2
ethyl-diphenyl-phosphane

: 71564-17-5,15651-51-1
manganese pentacarbonyl

: 47315-22-0
(CO)4Mn(P(C₆H₅)2(C₂H₅))

: 61943-36-0
HMn(CO)3(P(C₆H₅)2(C₂H₅))2

Guidance literature:: In not given; Irradiation (UV/VIS); under N2, irrdn. of educts in soln. with high-pressure Hg lamp (with cutoff UV35 filter) at 297 K; monitored by IR, ESR; Kinetics;
DOI:10.1016/0022-328X(83)80199-5