1,1'-bis(3'-methoxycarbonyl-4-biphenylyl)ferrocene

Base Information

Chemical Name:1,1'-bis(3'-methoxycarbonyl-4-biphenylyl)ferrocene
CAS No.:85129-62-0
Molecular Formula:C₃₈H₃₀FeO₄
Molecular Weight:606.501
Hs Code.:

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Chemical Property of 1,1'-bis(3'-methoxycarbonyl-4-biphenylyl)ferrocene

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Technology Process of 1,1'-bis(3'-methoxycarbonyl-4-biphenylyl)ferrocene

There total 1 articles about 1,1'-bis(3'-methoxycarbonyl-4-biphenylyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 102-54-5,55404-68-7
ferrocene

: 85096-04-4
4'-amino[1,1'-biphenyl]-3-carboxylic acid

: 85129-62-0
1,1'-bis(3'-methoxycarbonyl-4-biphenylyl)ferrocene

: 85129-63-1
(3'-methoxycarbonyl-4-biphenylyl)ferrocene

Guidance literature:: With methanol; sulfuric acid; sodium nitrite; In methanol; acetic acid; the amine diazotized in 10% H2SO4 at 0-5°C with NaNO2, added rapidly to soln. of Cp2Fe in AcOH under N2, stirred overnight at room temp., poured into water, (i), esterified in refluxing MeOH contg. concd. H2SO4 under N2, (ii); (i) ppt. filtered off, washed with water, dried at room temp.; (ii) evapd. in vac., extd. with CHCl3, washed with 5% NaHCO3 and brine, dried over MgSO4, filtered, concd., chromd. (SiO2, benzene); elem. anal.;
DOI:10.1246/bcsj.56.192