C₅₀H₅₄O₄Si

Base Information

Chemical Name:C₅₀H₅₄O₄Si
CAS No.:1452372-90-5
Molecular Formula:C₅₀H₅₄O₄Si
Molecular Weight:747.062
Hs Code.:

C<sub>50</sub>H<sub>54</sub>O<sub>4</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₀H₅₄O₄Si

Chemical Property:

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Technology Process of C₅₀H₅₄O₄Si

There total 7 articles about C₅₀H₅₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1452372-87-0
C₅₀H₅₄O₃Si

: 1452372-90-5
C₅₀H₅₄O₄Si

Guidance literature:: With Shi's ketone; oxone||potassium monopersulfate triple salt; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; potassium hydroxide; In acetonitrile;
DOI:10.3762/bjoc.9.132

Reference yield:

: 1452372-81-4
C₅₃H₅₉NO₄Si

: 1452372-90-5
C₅₀H₅₄O₄Si

Guidance literature:: Multi-step reaction with 3 steps

1: lithium amidotrihydridoborate / tetrahydrofuran / 0 - 20 °C

2: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran

3: Shi's ketone; oxone||potassium monopersulfate triple salt; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; potassium hydroxide / acetonitrile

With Shi's ketone; lithium amidotrihydridoborate; oxone||potassium monopersulfate triple salt; tetra(n-butyl)ammonium hydrogensulfate; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; potassium hydroxide; In tetrahydrofuran; acetonitrile; 3: |Shi Asymmetric Epoxidation;
DOI:10.3762/bjoc.9.132

Reference yield:

: 142096-78-4
(E)-1-hydroxy-4-(triphenylmethoxy)-2-butene

: 1452372-90-5
C₅₀H₅₄O₄Si

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

2: sodium iodide / acetone / 18 h / Darkness; Reflux; Inert atmosphere

3: lithium chloride; lithium diisopropyl amide / tetrahydrofuran

4: lithium amidotrihydridoborate / tetrahydrofuran / 0 - 20 °C

5: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran

6: Shi's ketone; oxone||potassium monopersulfate triple salt; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; potassium hydroxide / acetonitrile

With Shi's ketone; lithium amidotrihydridoborate; oxone||potassium monopersulfate triple salt; tetra(n-butyl)ammonium hydrogensulfate; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; triethylamine; sodium iodide; lithium chloride; potassium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; acetone; acetonitrile; 3: |Myers's Alkylation / 6: |Shi Asymmetric Epoxidation;
DOI:10.3762/bjoc.9.132