tetraphenylarsonium dichloro(phenylazoacetaldoximato)palladate(II)

Base Information

Chemical Name:tetraphenylarsonium dichloro(phenylazoacetaldoximato)palladate(II)
CAS No.:75687-19-3
Molecular Formula:C₈H₈Cl₂N₃OPd*C₂₄H₂₀As
Molecular Weight:722.841
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraphenylarsonium dichloro(phenylazoacetaldoximato)palladate(II)

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Technology Process of tetraphenylarsonium dichloro(phenylazoacetaldoximato)palladate(II)

There total 3 articles about tetraphenylarsonium dichloro(phenylazoacetaldoximato)palladate(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: di-μ-chlorobis[α-phenylazoacetaldoximato-N,N''palladium(II)]

: 507-28-8,14842-08-1
tetraphenylarsonium chloride

: 75687-19-3
tetraphenylarsonium dichloro(phenylazoacetaldoximato)palladate(II)

Guidance literature:: In dichloromethane; mixt. stirred for 15 min at 298 K; soln. completely evapd., gum dissolved in hot benzene-hexane mixt., evapn. in air yielded crystals which filtered off, washed with hexane, dried in air; elem. anal.;
DOI:10.1039/DT9800001698

Reference yield:

: 63056-54-2
bis(phenylazoacetaldoximato)palladium(II)

: 75687-19-3
tetraphenylarsonium dichloro(phenylazoacetaldoximato)palladate(II)

Guidance literature:: Multi-step reaction with 2 steps

1: Cl₂; ethanol / benzene

2: dichloromethane

With Cl₂; ethanol; In dichloromethane; benzene;
DOI:10.1039/DT9800001698

Reference yield:

: phenyldiazenylacetaldoxime

: 75687-19-3
tetraphenylarsonium dichloro(phenylazoacetaldoximato)palladate(II)

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol

2: dichloromethane

In ethanol; dichloromethane;
DOI:10.1039/DT9800001698