C₁₁H₁₆O₂

Base Information

Chemical Name:C₁₁H₁₆O₂
CAS No.:1432505-69-5
Molecular Formula:C₁₁H₁₆O₂
Molecular Weight:180.247
Hs Code.:

C<sub>11</sub>H<sub>16</sub>O<sub>2</sub>

Synonyms:

Suppliers and Price of C₁₁H₁₆O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₁₆O₂

Chemical Property:

Purity/Quality:

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Technology Process of C₁₁H₁₆O₂

There total 3 articles about C₁₁H₁₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1432505-67-3
C₁₂H₁₆O₄

: 1432505-69-5
C₁₁H₁₆O₂

: C₁₁H₁₆O₂

Guidance literature:: With (S)-2-(2-(bis(4-trifluoromethyl-phenyl)-phosphino))-5-(4-trifluoromethyl-phenyl)-4-tert-butyl-4,5-dihydro-oxazole; t r i s ( 4 , 4 ’-methoxydibenzylideneacetone)dipalladium(0); In toluene; at 40 ℃; for 144h; Overall yield = 99 %; Overall yield = 111 mg; enantioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1002/chem.201300030

Reference yield:

: 50741-71-4
2-benzyloxy-cyclohex-2-en-1-one

: 1432505-69-5
C₁₁H₁₆O₂

: C₁₁H₁₆O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: caesium carbonate / acetonitrile / 8 h / 80 °C / Inert atmosphere; Sealed tube

3.1: (S)-2-(2-(bis(4-trifluoromethyl-phenyl)-phosphino))-5-(4-trifluoromethyl-phenyl)-4-tert-butyl-4,5-dihydro-oxazole; t r i s ( 4 , 4 ’-methoxydibenzylideneacetone)dipalladium(0) / toluene / 144 h / 40 °C / Inert atmosphere; Sealed tube

With (S)-2-(2-(bis(4-trifluoromethyl-phenyl)-phosphino))-5-(4-trifluoromethyl-phenyl)-4-tert-butyl-4,5-dihydro-oxazole; t r i s ( 4 , 4 ’-methoxydibenzylideneacetone)dipalladium(0); caesium carbonate; lithium diisopropyl amide; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1002/chem.201300030

Reference yield:

: C₁₇H₁₈O₄

: 1432505-69-5
C₁₁H₁₆O₂

: C₁₁H₁₆O₂

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / acetonitrile / 8 h / 80 °C / Inert atmosphere; Sealed tube

2: (S)-2-(2-(bis(4-trifluoromethyl-phenyl)-phosphino))-5-(4-trifluoromethyl-phenyl)-4-tert-butyl-4,5-dihydro-oxazole; t r i s ( 4 , 4 ’-methoxydibenzylideneacetone)dipalladium(0) / toluene / 144 h / 40 °C / Inert atmosphere; Sealed tube

With (S)-2-(2-(bis(4-trifluoromethyl-phenyl)-phosphino))-5-(4-trifluoromethyl-phenyl)-4-tert-butyl-4,5-dihydro-oxazole; t r i s ( 4 , 4 ’-methoxydibenzylideneacetone)dipalladium(0); caesium carbonate; In toluene; acetonitrile;
DOI:10.1002/chem.201300030