9H-Xanthene-9-thiol, 9-(4-methoxyphenyl)-

Base Information

Chemical Name:9H-Xanthene-9-thiol, 9-(4-methoxyphenyl)-
CAS No.:132628-15-0
Molecular Formula:C20H16O2S
Molecular Weight:320.412
Hs Code.:
DSSTox Substance ID:DTXSID00564450
Wikidata:Q82449140

Synonyms:9-(4-METHOXYPHENYL)-9H-XANTHENE-9-THIOL;132628-15-0;9-(4-methoxyphenyl)xanthene-9-thiol;SCHEMBL5584000;DTXSID00564450

Suppliers and Price of 9H-Xanthene-9-thiol, 9-(4-methoxyphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 9H-Xanthene-9-thiol, 9-(4-methoxyphenyl)-

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:320.08710092
Heavy Atom Count:23
Complexity:382

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2(C3=CC=CC=C3OC4=CC=CC=C42)S

Technology Process of 9H-Xanthene-9-thiol, 9-(4-methoxyphenyl)-

There total 3 articles about 9H-Xanthene-9-thiol, 9-(4-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 94465-25-5
9-(4-methoxyphenyl)-9H-xanthen-9-ol

: 132628-15-0
9-(4-methoxyphenyl)-9H-xanthene-9-thiol

Guidance literature:: With dichloro-acetic acid; hydrogen sulfide; In dichloromethane; at 0 ℃;
DOI:10.1016/S0040-4039(00)88523-8

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 132628-15-0
9-(4-methoxyphenyl)-9H-xanthene-9-thiol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Mg, MeI / 1) ether, reflux, 1 h, 2) ether, reflux, 2 h

2: 88.5 percent / dichloroacetic acid, H₂S / CH₂Cl₂ / 0.25 h

With dichloro-acetic acid; hydrogen sulfide; magnesium; methyl iodide; In dichloromethane;
DOI:10.1016/0008-6215(92)84167-Q

Reference yield:

: 90-47-1
xanth-9-one

: 132628-15-0
9-(4-methoxyphenyl)-9H-xanthene-9-thiol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Mg, MeI / 1) ether, reflux, 1 h, 2) ether, reflux, 2 h

2: 88.5 percent / dichloroacetic acid, H₂S / CH₂Cl₂ / 0.25 h

With dichloro-acetic acid; hydrogen sulfide; magnesium; methyl iodide; In dichloromethane;
DOI:10.1016/0008-6215(92)84167-Q