Technology Process of C32H54O7
There total 4 articles about C32H54O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 98 percent / TPAP, 4-methylmorpholine N-oxide, 4A MS / CH2Cl2 / 4 h / 20 °C
2: 1.) sec-BuLi, 3.) MeI / 1.) THF, -95 deg C, 15 min, 2.) THF, -95 -> 20 deg C, 3.) THF/MeOH, 20 deg C, 1 h
3: 1.2N aq. HCl / tetrahydrofuran / 0.5 h / Heating
4: 1.) t-BuLi / 1.) hexane/Et2O, -78 deg C, 15 min, 2.) hexane/Et2O, -78 deg C, 1 h
With
hydrogenchloride; tetrapropylammonium perruthennate; tert.-butyl lithium; sec.-butyllithium; 4-methylmorpholine N-oxide; methyl iodide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(99)00367-6
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.2N aq. HCl / tetrahydrofuran / 0.5 h / Heating
2: 1.) t-BuLi / 1.) hexane/Et2O, -78 deg C, 15 min, 2.) hexane/Et2O, -78 deg C, 1 h
With
hydrogenchloride; tert.-butyl lithium;
In
tetrahydrofuran;
DOI:10.1016/S0040-4039(99)00367-6
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) sec-BuLi, 3.) MeI / 1.) THF, -95 deg C, 15 min, 2.) THF, -95 -> 20 deg C, 3.) THF/MeOH, 20 deg C, 1 h
2: 1.2N aq. HCl / tetrahydrofuran / 0.5 h / Heating
3: 1.) t-BuLi / 1.) hexane/Et2O, -78 deg C, 15 min, 2.) hexane/Et2O, -78 deg C, 1 h
With
hydrogenchloride; tert.-butyl lithium; sec.-butyllithium; methyl iodide;
In
tetrahydrofuran;
DOI:10.1016/S0040-4039(99)00367-6
