Technology Process of C34H31Cl2N3OS
There total 7 articles about C34H31Cl2N3OS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium methylate / butan-1-ol / 15 h / 140 °C
2: phosphorus pentachloride / dichloromethane / 4 h / Reflux
3: ammonium hydroxide / acetone / 0.5 h / 0 - 15 °C
4: tetraphosphorus decasulfide / tetrahydrofuran / 4 h / 50 - 55 °C
5: 3 h / Reflux
6: potassium carbonate / Reflux
With
ammonium hydroxide; tetraphosphorus decasulfide; phosphorus pentachloride; sodium methylate; potassium carbonate;
In
tetrahydrofuran; dichloromethane; acetone; butan-1-ol;
DOI:10.1007/s00044-012-0195-7
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium methylate / butan-1-ol / 15 h / 140 °C
2: phosphorus pentachloride / dichloromethane / 4 h / Reflux
3: ammonium hydroxide / acetone / 0.5 h / 0 - 15 °C
4: tetraphosphorus decasulfide / tetrahydrofuran / 4 h / 50 - 55 °C
5: 3 h / Reflux
6: potassium carbonate / Reflux
With
ammonium hydroxide; tetraphosphorus decasulfide; phosphorus pentachloride; sodium methylate; potassium carbonate;
In
tetrahydrofuran; dichloromethane; acetone; butan-1-ol;
DOI:10.1007/s00044-012-0195-7