[Fe(salpet)Cl]

Base Information

• Chemical Name: [Fe(salpet)Cl]
• CAS No.: 944797-47-1
• Molecular Formula: C₁₉H₂₁N₃O₂*Cl*Fe
• Molecular Weight: 414.695
• Mol file: 944797-47-1.mol

Synonyms:

Chemical Property of [Fe(salpet)Cl]

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [Fe(salpet)Cl]

There total 1 articles about [Fe(salpet)Cl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

iron(III) chloride hexahydrate (121714-78-1,24290-40-2,58694-80-7,10025-77-1,64333-00-2) + N,N'-bis(1-hydroxy-2-benzyliden) 1,6-diamino-3-azahexane (216772-98-4) → [Fe(salpet)Cl] (1192272-25-5,944797-47-1)

Guidance literature:

With triethyl amine; In methanol; a methanol soln. of amine-compound was combined with a methanol soln. ofFe-salt, triethylamine was added, stirred for 30 min at 50°C, co oled to room temp.; filtered, washed with cold methanol and diethyl ether; elem. anal.;

DOI:10.1039/b919120h

Reference yield: 79.0%

(N,N'-bis(1-hydroxy-2-benzyliden) 1,6-diamino-3-azahexane(-2H))FeCl (1192272-25-5,944797-47-1) + 3Ba(2+)*Fe(CN)5CNCo(CN)5(6-)=Ba3(CN)5FeCNCo(CN)5 → [((N,N'-bis(1-hydroxy-2-benzyliden) 1,6-diamino-3-azahexane(-2H))Fe(III)NC)10(Fe(II)CNCo(III))]Cl4

Guidance literature:

In methanol; water; CH3OH soln. of FeCl-compound combined with aq.-CH3OH 1:1 soln. of Ba-compound; stirred for 30 min; 60% of solvent evapd. using rotary evaporator at temp. less than 35°C; water added; cooled; filtered using Fritta IV filter; cleaned withcold water and Et2O; dried under vacuum for 24 h; filtered off; washed twice with MeOH; dried under Ar;

DOI:10.1016/j.poly.2006.11.041

upstream raw materials:

iron(III) chloride hexahydrate

N,N'-bis(1-hydroxy-2-benzyliden) 1,6-diamino-3-azahexane