1,2-Dihydroacenaphtho[3,4-b]benzo[d]thiophene

Base Information

Chemical Name:1,2-Dihydroacenaphtho[3,4-b]benzo[d]thiophene
CAS No.:18109-42-7
Molecular Formula:C17H17 N O
Molecular Weight:251.328
Hs Code.:
NSC Number:33399
DSSTox Substance ID:DTXSID10283786
Wikidata:Q82018481

Synonyms:1,2-dihydroacenaphtho[3,4-b]benzo[d]thiophene;NSC33399;DTXSID10283786;NSC-33399

Suppliers and Price of 1,2-Dihydroacenaphtho[3,4-b]benzo[d]thiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,2-Dihydroacenaphtho[3,4-b]benzo[d]thiophene

Chemical Property:

Vapor Pressure:5.49E-08mmHg at 25°C
Boiling Point:441.3°C at 760 mmHg
Flash Point:267.9°C
Density:1.122g/cm³
XLogP3:5.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:260.06597156
Heavy Atom Count:19
Complexity:365

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=C3C1=CC=CC3=CC4=C2SC5=CC=CC=C54

Technology Process of 1,2-Dihydroacenaphtho[3,4-b]benzo[d]thiophene

There total 6 articles about 1,2-Dihydroacenaphtho[3,4-b]benzo[d]thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 621-82-9
Cinnamic acid

: 87-62-7
2,6-dimethylaniline

: 18109-42-7
N-(2,6-dimethylphenyl)-cinnamamide

Guidance literature:: Cinnamic acid; With thionyl chloride; In N,N-dimethyl-formamide; toluene; at 0 ℃; for 2h; Reflux;

2,6-dimethylaniline; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1002/anie.201805641