2,3-Diamino-2,3-didesoxy-muco-inosit, Dihydrochlorid

Base Information

Chemical Name:2,3-Diamino-2,3-didesoxy-muco-inosit, Dihydrochlorid
CAS No.:80178-10-5
Molecular Formula:C₆H₁₄N₂O₄*2ClH
Molecular Weight:251.11
Hs Code.:

Synonyms:

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Chemical Property of 2,3-Diamino-2,3-didesoxy-muco-inosit, Dihydrochlorid

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Technology Process of 2,3-Diamino-2,3-didesoxy-muco-inosit, Dihydrochlorid

There total 6 articles about 2,3-Diamino-2,3-didesoxy-muco-inosit, Dihydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25876-20-4,90057-15-1
trans-6-Acetamido-5-acetoxy-1,3-cyclohexadien

: 80178-10-5,90129-54-7,110013-87-1,116127-32-3
1,2-Diamino-1,2-didesoxy-DL-chiro-inosit

Guidance literature:: Multi-step reaction with 4 steps

1: 55 percent / 1-Chlor-1-nitrosocyclohexan / ethanol; hexane / 504 h / -22 °C

2: 1) conc. HCl / Zn / 1) water, 2h, 0 deg C, 2) pyridin, 20h, room temp.; 80 deg C

3: 1) MgSO₄, KMnO₄ / 1) ethanol, water, 12h, room temp., 2) pyridin, 12h, 25 deg C

4: HCl / methanol / 7 h / Heating

With hydrogenchloride; potassium permanganate; 1-chloro-1-nitrosocyclohexane; magnesium sulfate; zinc; In methanol; ethanol; hexane;

Reference yield:

: 24664-86-6,90057-14-0
trans-6-Amino-5-hydroxy-1,3-cyclohexadien

: 80178-10-5,90129-54-7,110013-87-1,116127-32-3
1,2-Diamino-1,2-didesoxy-DL-chiro-inosit

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / 4-(Dimethylamino)pyridin, pyridin / diethyl ether / 3 h / Ambient temperature

2: 55 percent / 1-Chlor-1-nitrosocyclohexan / ethanol; hexane / 504 h / -22 °C

3: 1) conc. HCl / Zn / 1) water, 2h, 0 deg C, 2) pyridin, 20h, room temp.; 80 deg C

4: 1) MgSO₄, KMnO₄ / 1) ethanol, water, 12h, room temp., 2) pyridin, 12h, 25 deg C

5: HCl / methanol / 7 h / Heating

With pyridine; hydrogenchloride; dmap; potassium permanganate; 1-chloro-1-nitrosocyclohexane; magnesium sulfate; zinc; In methanol; diethyl ether; ethanol; hexane;

Reference yield:

: 90057-17-3
<8-exo,7-endo>-8-Acetamido-7-acetoxy-2-oxa-3-azabicyclo<2.2.2>oct-5-en-hydrochlorid

: 80178-10-5,90129-54-7,110013-87-1,116127-32-3
1,2-Diamino-1,2-didesoxy-DL-chiro-inosit

Guidance literature:: Multi-step reaction with 3 steps

1: 1) conc. HCl / Zn / 1) water, 2h, 0 deg C, 2) pyridin, 20h, room temp.; 80 deg C

2: 1) MgSO₄, KMnO₄ / 1) ethanol, water, 12h, room temp., 2) pyridin, 12h, 25 deg C

3: HCl / methanol / 7 h / Heating

With hydrogenchloride; potassium permanganate; magnesium sulfate; zinc; In methanol;