1,4',5-trimethyl-1,2,3,6-tetrahydro-1,1'-biphenyl

Base Information

Chemical Name:1,4',5-trimethyl-1,2,3,6-tetrahydro-1,1'-biphenyl
CAS No.:882876-36-0
Molecular Formula:C₁₅H₂₀
Molecular Weight:200.324
Hs Code.:

Synonyms:

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Chemical Property of 1,4',5-trimethyl-1,2,3,6-tetrahydro-1,1'-biphenyl

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1,4',5-trimethyl-1,2,3,6-tetrahydro-1,1'-biphenyl

There total 16 articles about 1,4',5-trimethyl-1,2,3,6-tetrahydro-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 882745-49-5
5-methyl-5-p-tolyl-cyclohex-3-enol

: 882876-36-0,761441-49-0
1,4',5-trimethyl-1,2,3,6-tetrahydro-1,1'-biphenyl

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / pyridinium chlorochromate; silica gel / CH₂Cl₂ / 3 h

2: 100 percent / H₂ / Pd/C / ethanol / 4 h / 760 Torr

3: 100 percent / diethyl ether / 0.5 h / 0 °C

4: phosphorous oxychloride; pyridine / CH₂Cl₂ / 2 h / 0 °C

With pyridine; hydrogen; silica gel; pyridinium chlorochromate; trichlorophosphate; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane;

Reference yield:

: 882745-50-8
5-(4-methylphenyl)-5-methylcyclohex-3-enone

: 882876-36-0,761441-49-0
1,4',5-trimethyl-1,2,3,6-tetrahydro-1,1'-biphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / Pd/C / ethanol / 4 h / 760 Torr

2: 100 percent / diethyl ether / 0.5 h / 0 °C

3: phosphorous oxychloride; pyridine / CH₂Cl₂ / 2 h / 0 °C

With pyridine; hydrogen; trichlorophosphate; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane;

Reference yield:

: 882745-48-4
6-methyl-6-p-tolyl-octa-1,7-dien-4-ol

: 882876-36-0,761441-49-0
1,4',5-trimethyl-1,2,3,6-tetrahydro-1,1'-biphenyl

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / [PhCH=Ru(Cl)2(PCy₃)2] / CH₂Cl₂ / 9 h / Heating

2: 95 percent / pyridinium chlorochromate; silica gel / CH₂Cl₂ / 3 h

3: 100 percent / H₂ / Pd/C / ethanol / 4 h / 760 Torr

4: 100 percent / diethyl ether / 0.5 h / 0 °C

5: phosphorous oxychloride; pyridine / CH₂Cl₂ / 2 h / 0 °C

With pyridine; hydrogen; silica gel; pyridinium chlorochromate; trichlorophosphate; Grubbs catalyst first generation; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane;