1-<3-<3-(p-nitrophenoxycarbonyl)propionamido>propylphosphinicomethyl>-1,4,7,10-tetraazacyclododecane-4,7,10-triyltris

Base Information

• Chemical Name: 1-<3-<3-(p-nitrophenoxycarbonyl)propionamido>propylphosphinicomethyl>-1,4,7,10-tetraazacyclododecane-4,7,10-triyltris
• CAS No.: 141380-96-3
• Molecular Formula: C₂₈H₅₂N₆O₁₃P₄
• Molecular Weight: 804.648

Synonyms:

Chemical Property of 1-<3-<3-(p-nitrophenoxycarbonyl)propionamido>propylphosphinicomethyl>-1,4,7,10-tetraazacyclododecane-4,7,10-triyltris

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-<3-<3-(p-nitrophenoxycarbonyl)propionamido>propylphosphinicomethyl>-1,4,7,10-tetraazacyclododecane-4,7,10-triyltris

There total 4 articles about 1-<3-<3-(p-nitrophenoxycarbonyl)propionamido>propylphosphinicomethyl>-1,4,7,10-tetraazacyclododecane-4,7,10-triyltris which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

succinic acid bis(p-nitrophenyl ester) (33109-58-9) + (3-Amino-propyl)-[4,7,10-tris-(hydroxy-methyl-phosphinoylmethyl)-1,4,7,10-tetraaza-cyclododec-1-ylmethyl]-phosphinic acid (138999-89-0) → 1-<3-<3-(p-nitrophenoxycarbonyl)propionamido>propylphosphinicomethyl>-1,4,7,10-tetraazacyclododecane-4,7,10-triyltris (141380-96-3)

Guidance literature:

With 4-methyl-morpholine; In dimethyl sulfoxide; at 45 ℃; for 4h; Yield given;

DOI:10.1055/s-1992-34177

Reference yield:

1-<<(3-benzamidopropyl)ethoxyphosphoryl>methyl>-1,4,7,10-tetraazacyclododecane (138999-86-7) → 1-<3-<3-(p-nitrophenoxycarbonyl)propionamido>propylphosphinicomethyl>-1,4,7,10-tetraazacyclododecane-4,7,10-triyltris (141380-96-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 40 percent / molecular sieves (3 A) / tetrahydrofuran / 16 h / Heating

2: 6M HCl / Heating

3: N-methylmorpholine / dimethylsulfoxide / 4 h / 45 °C

With 4-methyl-morpholine; hydrogenchloride; 3 A molecular sieve; In tetrahydrofuran; dimethyl sulfoxide;

DOI:10.1055/s-1992-34177

Reference yield:

(3-Benzoylamino-propyl)-[4,7,10-tris-(ethoxy-methyl-phosphinoylmethyl)-1,4,7,10-tetraaza-cyclododec-1-ylmethyl]-phosphinic acid ethyl ester (138999-87-8) → 1-<3-<3-(p-nitrophenoxycarbonyl)propionamido>propylphosphinicomethyl>-1,4,7,10-tetraazacyclododecane-4,7,10-triyltris (141380-96-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 6M HCl / Heating

2: N-methylmorpholine / dimethylsulfoxide / 4 h / 45 °C

With 4-methyl-morpholine; hydrogenchloride; In dimethyl sulfoxide;

DOI:10.1055/s-1992-34177

upstream raw materials:

succinic acid bis(p-nitrophenyl ester)

(3-Amino-propyl)-[4,7,10-tris-(hydroxy-methyl-phosphinoylmethyl)-1,4,7,10-tetraaza-cyclododec-1-ylmethyl]-phosphinic acid

1-<<(3-benzamidopropyl)ethoxyphosphoryl>methyl>-1,4,7,10-tetraazacyclododecane

(3-Benzoylamino-propyl)-[4,7,10-tris-(ethoxy-methyl-phosphinoylmethyl)-1,4,7,10-tetraaza-cyclododec-1-ylmethyl]-phosphinic acid ethyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 141380-96-3 1-<3-<3-(p-nitrophenoxycarbonyl)propionamido>propylphosphinicomethyl>-1,4,7,10-tetraazacyclododecane-4,7,10-triyltris

Send

Send

Metric Ton KG G Pound L ML

Send

Send