N-acetyllactosamine methyl glycoside

Base Information

Chemical Name:N-acetyllactosamine methyl glycoside
CAS No.:68774-40-3
Molecular Formula:C₁₅H₂₇NO₁₁
Molecular Weight:397.379
Hs Code.:

Synonyms:

Suppliers and Price of N-acetyllactosamine methyl glycoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of N-acetyllactosamine methyl glycoside

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of N-acetyllactosamine methyl glycoside

There total 1 articles about N-acetyllactosamine methyl glycoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3946-01-8
methyl N-acetyl-β-D-glucosaminide

: 3150-24-1
4-nitrophenyl-β-D-galactopyranoside

: 100836-88-2
Galβ(1-3)GlcNAcβ(1-)OCH3

: 68774-40-3
N-acetyllactosamine methyl glycoside

Guidance literature:: With sodium phosphate buffer pH 6.5; β-D-galactopyranoside; In N,N-dimethyl-formamide; at 37 ℃; for 1680h;
DOI:10.1016/0008-6215(89)84053-4

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 68774-40-3
N-acetyllactosamine methyl glycoside

: N-[(2R,3R,4R,5S,6R)-5-((4aR,6S,7R,8R,8aR)-7,8-Dihydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-4-hydroxy-6-hydroxymethyl-2-methoxy-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: With camphor-10-sulfonic acid; In N,N-dimethyl-formamide; at 50 ℃; for 2h;
DOI:10.1016/0008-6215(93)84251-Z

Reference yield:

: 68774-40-3
N-acetyllactosamine methyl glycoside

: 153756-68-4
methyl O-(6-deoxy-β-D-galactopyranosyl)-(1<*>4)-2-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 10 steps

1: camphorsulfonic acid / dimethylformamide / 2 h / 50 °C

2: DMAP / pyridine

3: 98 percent / 60percent aq.AcOH / 2 h / 90 °C

4: imidazole / dimethylformamide / 0.3 h / Ambient temperature

5: pyridine

6: 76 percent / 60percent aq.AcOH / 0.5 h / 90 °C

7: 77 percent / 4-dimethylaminopyridine, pyridine / 2 h / 50 °C

8: NaI / 1,2-dimethoxy-ethane / 12 h / 100 °C

9: Bu₃SnH, AIBN / 1,2-dimethoxy-ethane / 18 h / 100 °C

10: 93 percent / NaOMe / methanol / 3 h / Ambient temperature

With pyridine; 1H-imidazole; dmap; 2,2'-azobis(isobutyronitrile); camphor-10-sulfonic acid; tri-n-butyl-tin hydride; sodium methylate; acetic acid; sodium iodide; In pyridine; methanol; 1,2-dimethoxyethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(93)84251-Z