cyano-phenyl-maleic acid-anhydride

Base Information

Chemical Name:cyano-phenyl-maleic acid-anhydride
CAS No.:99971-66-1
Molecular Formula:C₁₁H₅NO₃
Molecular Weight:199.166
Hs Code.:

Synonyms:

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Chemical Property of cyano-phenyl-maleic acid-anhydride

Chemical Property:

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Technology Process of cyano-phenyl-maleic acid-anhydride

There total 7 articles about cyano-phenyl-maleic acid-anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15206-55-0
methyl 2-oxo-2-phenylacetate

: 99971-66-1
cyano-phenyl-maleic acid-anhydride

Guidance literature:: Multi-step reaction with 3 steps

1: methylamine hydrochloride; sodium carbonate; methanol / 20 °C

2: methanolic KOH-solution

3: water

With methanol; potassium hydroxide; water; methylamine hydrochloride; sodium carbonate;

Reference yield:

: 611-73-4
Benzoylformic acid

: 99971-66-1
cyano-phenyl-maleic acid-anhydride

Guidance literature:: Multi-step reaction with 4 steps

1: hydrochloric acid

2: methylamine hydrochloride; sodium carbonate; methanol / 20 °C

3: methanolic KOH-solution

4: water

With hydrogenchloride; methanol; potassium hydroxide; water; methylamine hydrochloride; sodium carbonate;

Reference yield:

: 613-90-1
benzoyl cyanide

: 99971-66-1
cyano-phenyl-maleic acid-anhydride

Guidance literature:: Multi-step reaction with 3 steps

2: concentrated aqueous HCl

3: 144 - 148 °C

With hydrogenchloride;
DOI:10.1021/ja01544a057