quinuclidine-benzyl(ethylnitrilio)borane tetrafluoroborate

Base Information

Chemical Name:quinuclidine-benzyl(ethylnitrilio)borane tetrafluoroborate
CAS No.:125844-06-6
Molecular Formula:BF₄*C₁₆H₂₄BN₂
Molecular Weight:341.996
Hs Code.:

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Chemical Property of quinuclidine-benzyl(ethylnitrilio)borane tetrafluoroborate

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Technology Process of quinuclidine-benzyl(ethylnitrilio)borane tetrafluoroborate

There total 6 articles about quinuclidine-benzyl(ethylnitrilio)borane tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 124287-33-8
quinuclidine-benzylcyanoborane

: 368-39-8
triethyloxonium fluoroborate

: 125844-06-6
quinuclidine-benzyl(ethylnitrilio)borane tetrafluoroborate

Guidance literature:: In dichloromethane; under N2; soln. of borane tranferred to Et3OBF4, reaction complete after 1-4d, left overnight; evapd., added to H2O, extd. (CH2Cl2 or CHCl3), dried (Na2SO4), evapd.; elem. anal.;

Reference yield: 95.0%

: 124287-33-8
quinuclidine*BH(benzyl)CN

: 368-39-8
triethyloxonium fluoroborate

: 125844-06-6
{quinuclidine*BH(benzyl)-CNEt}⁽¹⁺⁾*BF₄^(1-)

Guidance literature:: treatment of (HC(CH2CH2)3N*BH(benzyl)CN with an excess of (Et3O)BF4 gave the nitrilium salt; elem. anal.;
DOI:10.1039/c39890000900

Reference yield:

: 124287-23-6
quinuclidine*BH₂-benzyl

: 125844-06-6
{quinuclidine*BH(benzyl)-CNEt}⁽¹⁺⁾*BF₄^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1: I₂ / benzene

2: NaCN / tetrahydrofuran

With I₂; NaCN; In tetrahydrofuran; benzene;
DOI:10.1039/c39890000900