2-benzyl-3,4-dimethylphosphacymantrene

Base Information

Chemical Name:2-benzyl-3,4-dimethylphosphacymantrene
CAS No.:444178-05-6
Molecular Formula:C₁₆H₁₄MnO₃P
Molecular Weight:340.197
Hs Code.:

Synonyms:

Suppliers and Price of 2-benzyl-3,4-dimethylphosphacymantrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-benzyl-3,4-dimethylphosphacymantrene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-benzyl-3,4-dimethylphosphacymantrene

There total 1 articles about 2-benzyl-3,4-dimethylphosphacymantrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 68079-65-2
2-benzoly-3,4-dimethylphosphacymantrene

: 444178-05-6
2-benzyl-3,4-dimethylphosphacymantrene

: rac-(E)-2,3-bis[3',4'-dimethylphosphacymantren-2'-yl]-1,2-diphenylethene

Guidance literature:: With titanium tetrachloride; zinc; In tetrahydrofuran; under N2, Zn dust was placed in a Schlenk tube, C4H8O was added, TiCl4 was added at 0°C, the mixt. was refluxed for 2 h, a soln. of the phosphacymantrene in C4H8O was added, the mixt. was refluxed for 48 h; the mixt. was evapd. in vac., the residue was dissolved in (C2H5)2O, thesoln. was washed with aq. NaHCO3 and water, dried over MgSO4, filtered, evapd. in vac., the residue was chromd. (SiO2, hexane/(C2H5)2O); elem. anal.;
DOI:10.1021/om020144h