C₂₄H₂₃NO₄Se

Base Information

• Chemical Name: C₂₄H₂₃NO₄Se
• CAS No.: 1360573-52-9
• Molecular Formula: C₂₄H₂₃NO₄Se
• Molecular Weight: 468.411
• Mol file: 1360573-52-9.mol

Synonyms:

Chemical Property of C₂₄H₂₃NO₄Se

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₃NO₄Se

There total 1 articles about C₂₄H₂₃NO₄Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

3-(phenylseleno)propylamine (125424-56-8) + 4-formyl-3-hydroxyphenyl 4-methoxybenzoate (940880-67-1) → C24H23NO4Se (1360573-52-9)

Guidance literature:

In ethanol; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1039/c1dt11695a

Reference yield: 89.0%

sodium tetrachloropalladate(II) + C24H23NO4Se (1360573-52-9) → PdClC6H5Se(CH2)3NCHC6H3OCO2C6H4OCH3 (1360618-43-4)

Guidance literature:

In water; acetone; Na2PdCl4 dissolved in H2O, acetone soln. of ligand added with stirring, stirred for 2 h; extd. with CHCl3, CHCl3 layer washed with H2O, dried with Na2SO4, vol. reduced in vacuo, mixed with hexane; elem. anal.;

DOI:10.1039/c1dt11695a

upstream raw materials:

3-(phenylseleno)propylamine

4-formyl-3-hydroxyphenyl 4-methoxybenzoate

Downstream raw materials:

PdClC₆H₅Se(CH₂)3NCHC₆H₃OCO₂C₆H₄OCH₃