nitro-4 benzoate de tridesoxy-2,3,6 O-((dihydroxy-5,12 dioxo-6,11 methyl-1 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannyl-3-(1S,3S)) methyl)-1 trifluoroacetamido-3 L-arabino-hexopyrannose

Base Information

Chemical Name:nitro-4 benzoate de tridesoxy-2,3,6 O-((dihydroxy-5,12 dioxo-6,11 methyl-1 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannyl-3-(1S,3S)) methyl)-1 trifluoroacetamido-3 L-arabino-hexopyrannose
CAS No.:128885-78-9
Molecular Formula:C₃₄H₂₉F₃N₂O₁₂
Molecular Weight:714.606
Hs Code.:

nitro-4 benzoate de tridesoxy-2,3,6 O-((dihydroxy-5,12 dioxo-6,11 methyl-1 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannyl-3-(1S,3S)) methyl)-1 trifluoroacetamido-3 L-arabino-hexopyrannose

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Chemical Property of nitro-4 benzoate de tridesoxy-2,3,6 O-((dihydroxy-5,12 dioxo-6,11 methyl-1 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannyl-3-(1S,3S)) methyl)-1 trifluoroacetamido-3 L-arabino-hexopyrannose

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Technology Process of nitro-4 benzoate de tridesoxy-2,3,6 O-((dihydroxy-5,12 dioxo-6,11 methyl-1 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannyl-3-(1S,3S)) methyl)-1 trifluoroacetamido-3 L-arabino-hexopyrannose

There total 12 articles about nitro-4 benzoate de tridesoxy-2,3,6 O-((dihydroxy-5,12 dioxo-6,11 methyl-1 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannyl-3-(1S,3S)) methyl)-1 trifluoroacetamido-3 L-arabino-hexopyrannose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 73891-04-0
2,3,6-tridesoxy-4-O-p-nitrobenzoyl-3-(trifluoroacetamido)-L-arabino-hex-1-enitol

: 111407-71-7
(-)-(1S,3S)-dihydroxy-5,12 hydroxymethyl-3 methyl-1 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannedione-6,11

: 128885-78-9,128947-85-3,128947-86-4,128947-87-5
nitro-4 benzoate de tridesoxy-2,3,6 O-((dihydroxy-5,12 dioxo-6,11 methyl-1 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannyl-3-(1S,3S)) methyl)-1 trifluoroacetamido-3 L-arabino-hexopyrannose

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; benzene; at 50 ℃; for 2h;

Reference yield: 10.0%

: 73891-04-0
2,3,6-tridesoxy-4-O-p-nitrobenzoyl-3-(trifluoroacetamido)-L-arabino-hex-1-enitol

: 111301-53-2
(+)-(1R,3S)-dihydroxy-5,12 hydroxymethyl-3 methyl-1 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannedione-6,11

: 128885-78-9,128947-85-3,128947-86-4,128947-87-5
nitro-4 benzoate de tridesoxy-2,3,6 O-((dihydroxy-5,12 dioxo-6,11 methyl-1 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannyl-3-(1R,3S)) methyl)-1 trifluoroacetamido-3 L-arabino-hexopyrannose

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; benzene; at 50 ℃; for 2h;

Reference yield:

: 23861-72-5
ethyl-2 quinizarine

: 128885-78-9,128947-85-3,128947-86-4,128947-87-5
nitro-4 benzoate de tridesoxy-2,3,6 O-((dihydroxy-5,12 dioxo-6,11 methyl-1 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannyl-3-(1R,3S)) methyl)-1 trifluoroacetamido-3 L-arabino-hexopyrannose

Guidance literature:: Multi-step reaction with 6 steps

1: 16 percent / 0.3 N KOH, sodium bisulfite / methanol / 12 h / 40 °C

2: N HCl / methanol / 4 h / 20 °C

3: pyridine

4: 54 percent / dibromo-1,3 dimethyl-5,5 hydantoine / CCl₄ / 1 h / Irradiation

5: 30 percent / HCl gas / methanol / 3.5 h / Heating

6: 10 percent / p-toluenesulfonic acid / benzene; CH₂Cl₂ / 2 h / 50 °C

With hydrogenchloride; potassium hydroxide; dimethyldibromohydantoin; toluene-4-sulfonic acid; sodium hydrogensulfite; In pyridine; methanol; tetrachloromethane; dichloromethane; benzene;