7-chloro-3-methyl-7-phenyl-2-heptene

Base Information

Chemical Name:7-chloro-3-methyl-7-phenyl-2-heptene
CAS No.:56040-05-2
Molecular Formula:C₁₄H₁₉Cl
Molecular Weight:222.758
Hs Code.:

Synonyms:

Suppliers and Price of 7-chloro-3-methyl-7-phenyl-2-heptene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-chloro-3-methyl-7-phenyl-2-heptene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-chloro-3-methyl-7-phenyl-2-heptene

There total 7 articles about 7-chloro-3-methyl-7-phenyl-2-heptene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57253-27-7
(E)-4-methylhex-4-en-1-ol

: 56040-05-2
7-chloro-3-methyl-7-phenyl-2-heptene

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 2 h / 0 °C

2: anhydrous LiBr / acetone / 0.5 h / Heating

3: 46 percent / Li / tetrahydrofuran / Ambient temperature

4: 1.) hexamethylphosphoramide, CH₃Li, methanesulfonyl chloride, 2.) LiCl / 1.) anhydrous ether, hexamethylphosphoramide, 2.) room temp., 20 min

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; methyllithium; lithium; methanesulfonyl chloride; lithium chloride; lithium bromide; In tetrahydrofuran; acetone;
DOI:10.1021/jo00269a053

Reference yield:

: 71435-23-9
6-bromo-3-methyl-2-hexene

: 56040-05-2
7-chloro-3-methyl-7-phenyl-2-heptene

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / Li / tetrahydrofuran / Ambient temperature

2: 1.) hexamethylphosphoramide, CH₃Li, methanesulfonyl chloride, 2.) LiCl / 1.) anhydrous ether, hexamethylphosphoramide, 2.) room temp., 20 min

With N,N,N,N,N,N-hexamethylphosphoric triamide; methyllithium; lithium; methanesulfonyl chloride; lithium chloride; In tetrahydrofuran;
DOI:10.1021/jo00269a053

Reference yield:

: 58203-62-6
ethyl (E)-4-methylhex-4-enoate

: 56040-05-2
7-chloro-3-methyl-7-phenyl-2-heptene

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

2: pyridine / 2 h / 0 °C

3: anhydrous LiBr / acetone / 0.5 h / Heating

4: 46 percent / Li / tetrahydrofuran / Ambient temperature

5: 1.) hexamethylphosphoramide, CH₃Li, methanesulfonyl chloride, 2.) LiCl / 1.) anhydrous ether, hexamethylphosphoramide, 2.) room temp., 20 min

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; methyllithium; lithium; methanesulfonyl chloride; lithium chloride; lithium bromide; In tetrahydrofuran; diethyl ether; acetone;
DOI:10.1021/jo00269a053