{OsCl(PH₃)(NCCH₃)(CO)(PPh₃)2}ClO₄

Base Information

Chemical Name:{OsCl(PH₃)(NCCH₃)(CO)(PPh₃)2}ClO₄
CAS No.:116890-88-1
Molecular Formula:C₃₉H₃₆ClNOOsP₃*ClO₄
Molecular Weight:952.746
Hs Code.:

{OsCl(PH<sub>3</sub>)(NCCH<sub>3</sub>)(CO)(PPh<sub>3</sub>)2}ClO<sub>4</sub>

Synonyms:

Suppliers and Price of {OsCl(PH₃)(NCCH₃)(CO)(PPh₃)2}ClO₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of {OsCl(PH₃)(NCCH₃)(CO)(PPh₃)2}ClO₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of {OsCl(PH₃)(NCCH₃)(CO)(PPh₃)2}ClO₄

There total 2 articles about {OsCl(PH₃)(NCCH₃)(CO)(PPh₃)2}ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: OsHCl(PH₃)(CO)(PPh₃)2*0.75CH₂Cl₂

: 75-05-8,26809-02-9
acetonitrile

: 116890-88-1,116890-87-0,103932-39-4
{OsCl(PH₃)(NCCH₃)(CO)(PPh₃)2}ClO₄

Guidance literature:: With HClO₄; In dichloromethane; water; Soln. of OsHCl(PH3)(CO)(PPh3)2 in CH2Cl2 treated with aq. soln. of 60% HClO4 in CH3CN, 2 h stirred at 25°C. Mixt. of isomers (54/32/14) obtained.; evapn.; recrystn. from dichlormethane/ethanol/isopropanol; elem. anal.;
DOI:10.1016/0022-328X(88)80421-2

Reference yield:

: 16971-31-6,36007-23-5
hydridocarbonylchlorotris(triphenylphosphine)osmium(II)

: 116890-88-1,116890-87-0,103932-39-4
{OsCl(PH₃)(NCCH₃)(CO)(PPh₃)2}ClO₄

Guidance literature:: Multi-step reaction with 2 steps

1: not given

2: HClO₄ / not given

With HClO₄; In not given;
DOI:10.1039/c39850001594

Reference yield: 99.0%

: 116890-88-1,116890-87-0,103932-39-4
{OsCl(PH₃)(NCCH₃)(CO)(PPh₃)2}ClO₄

: 594-09-2
trimethylphosphane

: 116890-90-5,116949-84-9
OsCl(PH₃)(P(CH₃)3)(CO)(P(C₆H₅)3)2⁽¹⁺⁾*ClO₄^(1-)

Guidance literature:: In tetrahydrofuran; benzene; OsCl(PH3)(NCCH3)(CO)(PPh3)2ClO4 suspended in THF was treated with a two-fold excess of trimethylphosphine in benzene soln., stirred for 30 min and THF removed in vacuo. Mixt. of isomers obtained.; washing with ethanol and hexane; elem. anal.;
DOI:10.1016/0022-328X(88)80421-2