2-Methoxy-1-nitro-4-(propylsulfanyl)benzene

Base Information

Chemical Name:2-Methoxy-1-nitro-4-(propylsulfanyl)benzene
CAS No.:132992-53-1
Molecular Formula:C₁₀H₁₃NO₃S
Molecular Weight:227.284
Hs Code.:
DSSTox Substance ID:DTXSID10569012
Wikidata:Q82455705

Synonyms:132992-53-1;2-Methoxy-1-nitro-4-(propylsulfanyl)benzene;DTXSID10569012

Suppliers and Price of 2-Methoxy-1-nitro-4-(propylsulfanyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Methoxy-1-nitro-4-(propylsulfanyl)benzene

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:227.06161445
Heavy Atom Count:15
Complexity:207

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCSC1=CC(=C(C=C1)[N+](=O)[O-])OC

Technology Process of 2-Methoxy-1-nitro-4-(propylsulfanyl)benzene

There total 1 articles about 2-Methoxy-1-nitro-4-(propylsulfanyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107-03-9
1-thiopropane

: 6627-53-8
1-chloro-3-methoxy-4-nitrobenzene

: 132992-53-1
2-nitro-5-propylthioanisole

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, ice bath, 40 min., 2.) DMF, ice bath, 2 h;
DOI:10.1248/cpb.40.351

Reference yield: 52.0%

: 132992-53-1
2-nitro-5-propylthioanisole

: 132992-52-0
4-propylthio-o-anisidine

Guidance literature:: With sodium dithionite; In methanol; water; for 0.166667h; Heating;
DOI:10.1248/cpb.40.351

Reference yield:

: 132992-53-1
2-nitro-5-propylthioanisole

: 136063-52-0
2-methoxy-N-methyl-4-(propylthio)acetanilide

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / Na₂S₂O₄ / H₂O; methanol / 0.17 h / Heating

2: 97 percent / Et₃N / CH₂Cl₂ / 9 h / Ambient temperature

3: 1.) NaH / 1.) DMF, 0.5 h, 2.) DMF, 5.5 h

With sodium dithionite; sodium hydride; triethylamine; In methanol; dichloromethane; water;
DOI:10.1248/cpb.40.351