C₂₇H₂₉⁽²⁾H₂N₃O₆

Base Information

Chemical Name:C₂₇H₂₉⁽²⁾H₂N₃O₆
CAS No.:1373889-11-2
Molecular Formula:C₂₇H₃₁N₃O₆
Molecular Weight:495.544
Hs Code.:

C<sub>27</sub>H<sub>29</sub><sup>(2)</sup>H<sub>2</sub>N<sub>3</sub>O<sub>6</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₉⁽²⁾H₂N₃O₆

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Technology Process of C₂₇H₂₉⁽²⁾H₂N₃O₆

There total 6 articles about C₂₇H₂₉⁽²⁾H₂N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1373889-08-7
C₄₃H₄₇⁽²⁾H₂N₃O₆Si

: 1373889-11-2
C₂₇H₂₉⁽²⁾H₂N₃O₆

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 18h;
DOI:10.1021/ja302711z

Reference yield:

: 1373889-06-5
C₁₈H₁₅⁽²⁾H₂NO₃

: 1373889-11-2
C₂₇H₂₉⁽²⁾H₂N₃O₆

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h

With tetrabutyl ammonium fluoride; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja302711z

Reference yield:

: 1373889-07-6
C₃₀H₄₂N₂O₆Si

: 1373889-11-2
C₂₇H₂₉⁽²⁾H₂N₃O₆

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 20 h

2: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h

With tetrabutyl ammonium fluoride; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja302711z