1-(triphenylphosphinegold(I))imidazole

Base Information

Chemical Name:1-(triphenylphosphinegold(I))imidazole
CAS No.:82092-59-9
Molecular Formula:C₂₁H₁₈AuN₂P
Molecular Weight:526.328
Hs Code.:

Synonyms:

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Chemical Property of 1-(triphenylphosphinegold(I))imidazole

Chemical Property:

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Technology Process of 1-(triphenylphosphinegold(I))imidazole

There total 4 articles about 1-(triphenylphosphinegold(I))imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 288-32-4
1H-imidazole

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 82092-59-9
1-(triphenylphosphinegold(I))imidazole

Guidance literature:: With tetra(n-butyl)ammonium hydrogensulfate; In sodium hydroxide; dichloromethane; soln. of the Au-complex and imidazole in CH2Cl2 mixed under stirring with an ice-cold soln. of tetrabutylammonium hydrogen sulphate in aq. NaOH, stirred for 2 h at room temp.; org. layer sepd., washed with water till neutral washing, dried over Na2SO4, evapd. to dryness under reduced pressure, extd. with benzene, concd., pptd. by addn. of petroleum ether, purified twice in the same way, MP, IR, NMR;

Reference yield:

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 82092-59-9
1-(triphenylphosphinegold(I))imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / water; tetrahydrofuran

2: chloroform

With KOH; In tetrahydrofuran; chloroform; water;
DOI:10.1246/bcsj.62.1078

Reference yield:

: 288-32-4
1H-imidazole

: (5-fluoro-2'-deoxyuridinato-N₃)(triphenylphosphine)gold(I)

: 82092-59-9
1-(triphenylphosphinegold(I))imidazole

Guidance literature:: In chloroform; the imidazole was added to a chloroform solution containing the complex; shaken vigorously for ten minutes; unreacted imidazol was extracted into the aqueous KOH phase; evaporation; 1H-NMR, IR;
DOI:10.1246/bcsj.62.1078