cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylarsane molybdenum(II)

Base Information

Chemical Name:cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylarsane molybdenum(II)
CAS No.:83328-24-9
Molecular Formula:C₂₈H₂₆AsBrMoO₂
Molecular Weight:645.279
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Chemical Property of cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylarsane molybdenum(II)

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Technology Process of cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylarsane molybdenum(II)

There total 2 articles about cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylarsane molybdenum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 12107-35-6
Na[CpMo(CO)3]

: 83206-32-0
(C₆H₅CH₂)3AsBr₂

: 83328-24-9
cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylarsane molybdenum(II)

Guidance literature:: In methyl cyclohexane; byproducts: NaBr, CO; (N2), to a susp. of Mo-complex in methylcyclohexane added organic compound in the same solvent, mixture heated at 60°C for 100 h; filtered, evaporated in vac., extracted with pentane/toluene (5:1), cooled to-78°C; elem. anal.;

Reference yield: 40.0%

: tricarbonylbromo(η-cyclopentadienyl)molybdenum

: 5888-61-9
tri-benzyl-arsine

: 83328-24-9
cis-bromo-dicarbonyl(η5-cyclopentadienyl)-trisbenzylarsane molybdenum(II)

Guidance literature:: In benzene; byproducts: CO; (N2), to the Mo-complex in benzene added organic compound in the same solvent, mixture heated at 50-60°C for 40 h; solvent removed in vac., (PhCH2)3As removed, filtered, evaporated in vac., extracted with pentane/toluene (5:1), cooled to -78°C; elem. anal.;