C₅₉H₇₇I₂NO

Base Information

Chemical Name:C₅₉H₇₇I₂NO
CAS No.:1416431-61-2
Molecular Formula:C₅₉H₇₇I₂NO
Molecular Weight:1070.08
Hs Code.:

C<sub>59</sub>H<sub>77</sub>I<sub>2</sub>NO

Synonyms:

Suppliers and Price of C₅₉H₇₇I₂NO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₉H₇₇I₂NO

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₅₉H₇₇I₂NO

There total 8 articles about C₅₉H₇₇I₂NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416431-65-6
icosa-5,7-diynyltosylate

: 1416431-61-2
C₅₉H₇₇I₂NO

Guidance literature:: Multi-step reaction with 6 steps

1: sodium azide / N,N-dimethyl-formamide / 3 h / 70 °C / Inert atmosphere

2: tin(ll) chloride / methanol / 4 h / 0 - 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

4: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

5: potassium hydroxide / methanol; tetrahydrofuran

6: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium azide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 4: |Sonogashira Cross-Coupling / 6: |Sonogashira Cross-Coupling;
DOI:10.1021/ja3116422

Reference yield:

: 174063-93-5
C₂₀H₃₄O

: 1416431-61-2
C₅₉H₇₇I₂NO

Guidance literature:: Multi-step reaction with 7 steps

1: dmap; triethylamine / dichloromethane / 2 h

2: sodium azide / N,N-dimethyl-formamide / 3 h / 70 °C / Inert atmosphere

3: tin(ll) chloride / methanol / 4 h / 0 - 20 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

5: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

6: potassium hydroxide / methanol; tetrahydrofuran

7: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium azide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 5: |Sonogashira Cross-Coupling / 7: |Sonogashira Cross-Coupling;
DOI:10.1021/ja3116422

Reference yield:

: 1416431-57-6
C₂₀H₃₃N₃

: 1416431-61-2
C₅₉H₇₇I₂NO

Guidance literature:: Multi-step reaction with 5 steps

1: tin(ll) chloride / methanol / 4 h / 0 - 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

3: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

4: potassium hydroxide / methanol; tetrahydrofuran

5: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; 3: |Sonogashira Cross-Coupling / 5: |Sonogashira Cross-Coupling;
DOI:10.1021/ja3116422