Technology Process of C21H17ClN4O
There total 4 articles about C21H17ClN4O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
isopropyl alcohol;
at 110 ℃;
Microwave irradiation;
DOI:10.1016/j.bmcl.2012.02.013
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 100 °C
2: Lawessons reagent / 100 °C
3: tert.-butylhydroperoxide; ammonium hydroxide
4: potassium carbonate / isopropyl alcohol / 110 °C / Microwave irradiation
With
Lawessons reagent; tert.-butylhydroperoxide; ammonium hydroxide; potassium carbonate;
In
isopropyl alcohol;
4: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.02.013
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium cyanide / 120 °C
2: 100 °C
3: Lawessons reagent / 100 °C
4: tert.-butylhydroperoxide; ammonium hydroxide
5: potassium carbonate / isopropyl alcohol / 110 °C / Microwave irradiation
With
Lawessons reagent; tert.-butylhydroperoxide; potassium cyanide; ammonium hydroxide; potassium carbonate;
In
isopropyl alcohol;
1: Bucherer-Bergs reaction / 5: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.02.013