tert-butyl(((2S,3S)-6-((tert-butyldimethylsilyl)oxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-((4-methoxybenzyl)oxy)-5-methylhex-1-en-1-yl)-3,6-dihydro-2H-pyran-3-yl)oxy)diphenylsilane

Base Information

• Chemical Name: tert-butyl(((2S,3S)-6-((tert-butyldimethylsilyl)oxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-((4-methoxybenzyl)oxy)-5-methylhex-1-en-1-yl)-3,6-dihydro-2H-pyran-3-yl)oxy)diphenylsilane
• CAS No.: 1240018-04-5
• Molecular Formula: C₄₆H₆₈O₇Si₂
• Molecular Weight: 789.213

Synonyms:

Chemical Property of tert-butyl(((2S,3S)-6-((tert-butyldimethylsilyl)oxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-((4-methoxybenzyl)oxy)-5-methylhex-1-en-1-yl)-3,6-dihydro-2H-pyran-3-yl)oxy)diphenylsilane

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Technology Process of tert-butyl(((2S,3S)-6-((tert-butyldimethylsilyl)oxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-((4-methoxybenzyl)oxy)-5-methylhex-1-en-1-yl)-3,6-dihydro-2H-pyran-3-yl)oxy)diphenylsilane

There total 1 articles about tert-butyl(((2S,3S)-6-((tert-butyldimethylsilyl)oxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-((4-methoxybenzyl)oxy)-5-methylhex-1-en-1-yl)-3,6-dihydro-2H-pyran-3-yl)oxy)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C30H50O7Si (1240018-03-4) + tert-butylchlorodiphenylsilane (58479-61-1) → tert-butyl(((2S,3S)-6-((tert-butyldimethylsilyl)oxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-((4-methoxybenzyl)oxy)-5-methylhex-1-en-1-yl)-3,6-dihydro-2H-pyran-3-yl)oxy)diphenylsilane (1240018-04-5)

Guidance literature:

With pyridine; silver nitrate; In dichloromethane; at 25 ℃; for 16h; Inert atmosphere; Darkness;

DOI:10.1021/jo1010203

Reference yield:

tert-butyl(((2S,3S)-6-((tert-butyldimethylsilyl)oxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-((4-methoxybenzyl)oxy)-5-methylhex-1-en-1-yl)-3,6-dihydro-2H-pyran-3-yl)oxy)diphenylsilane (1240018-04-5) → (5S,6S)-5-((tert-butyldiphenylsilyl)oxy)-6-((4S,5S,E)-4-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhex-1-en-1-yl)-5,6-dihydro-2H-pyran-2-ol (1240018-05-6)

Guidance literature:

With hydrogenchloride; water; In tetrahydrofuran; at 25 ℃; for 12h; Inert atmosphere;

DOI:10.1021/jo1010203

upstream raw materials:

C₃₀H₅₀O₇Si

tert-butylchlorodiphenylsilane

Downstream raw materials:

(5S,6S)-5-((tert-butyldiphenylsilyl)oxy)-6-((4S,5S,E)-4-hydroxy-6-((4-methoxybenzyl)oxy)-5-methylhex-1-en-1-yl)-5,6-dihydro-2H-pyran-2-ol

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