C₃₅H₃₃N₃O₃

Base Information

Chemical Name:C₃₅H₃₃N₃O₃
CAS No.:1415220-48-2
Molecular Formula:C₃₅H₃₃N₃O₃
Molecular Weight:543.665
Hs Code.:

C<sub>35</sub>H<sub>33</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

Suppliers and Price of C₃₅H₃₃N₃O₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₅H₃₃N₃O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₅H₃₃N₃O₃

There total 5 articles about C₃₅H₃₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54503-64-9,54503-65-0
2,3-O-isopropylidene-5-O-trityl-D-ribofuranose

: 1415220-48-2
C₃₅H₃₃N₃O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2.1: dmap; 1H-imidazole / dichloromethane; N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -60 °C / Inert atmosphere

3.2: 1 h / -60 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

4.2: 12 h / 0 - 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

6.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 20 °C / Inert atmosphere

7.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; n-butyllithium; oxalyl dichloride; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; dimethyl sulfoxide; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 7.1: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2012.09.072

Reference yield:

: 67814-68-0,70266-87-4,76249-50-8,76249-51-9,93451-15-1,4099-88-1
2,3-O-isopropylidene-D-ribofuranose

: 1415220-48-2
C₃₅H₃₃N₃O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: dmap; triethylamine / dichloromethane; N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

2.1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

3.1: dmap; 1H-imidazole / dichloromethane; N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -60 °C / Inert atmosphere

4.2: 1 h / -60 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

5.2: 12 h / 0 - 20 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

7.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 20 °C / Inert atmosphere

8.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; n-butyllithium; oxalyl dichloride; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; dimethyl sulfoxide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 8.1: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2012.09.072

Reference yield:

: 1-[5-(1-hydroxy-2-trityloxyethyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]prop-2-en-1-ol

: 1415220-48-2
C₃₅H₃₃N₃O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: dmap; 1H-imidazole / dichloromethane; N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -60 °C / Inert atmosphere

2.2: 1 h / -60 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.2: 12 h / 0 - 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

5.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 20 °C / Inert atmosphere

6.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; n-butyllithium; oxalyl dichloride; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; dimethyl sulfoxide; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 6.1: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2012.09.072