C₄₀H₅₇N₉O₈

Base Information

Chemical Name:C₄₀H₅₇N₉O₈
CAS No.:1356409-90-9
Molecular Formula:C₄₀H₅₇N₉O₈
Molecular Weight:791.948
Hs Code.:

C<sub>40</sub>H<sub>57</sub>N<sub>9</sub>O<sub>8</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₀H₅₇N₉O₈

Chemical Property:

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Technology Process of C₄₀H₅₇N₉O₈

There total 3 articles about C₄₀H₅₇N₉O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356409-08-9
C₁₈H₁₉NO₄

: 1356409-16-9
GSKFR

: 1356409-37-4
C₄₀H₅₇N₉O₈

: 1356409-90-9
C₄₀H₅₇N₉O₈

Guidance literature:: With chloro(meso-tetrakis(2,6-dichlorophenyl)porphyrinato)manganese(III); dihydrogen peroxide; sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃; for 0.25h; pH=6.3; aq. phosphate buffer;
DOI:10.1021/ja208009r

Reference yield:

: 101-41-7
benzeneacetic acid methyl ester

: 1356409-37-4
C₄₀H₅₇N₉O₈

: 1356409-90-9
C₄₀H₅₇N₉O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 1.5 h / -78 - 0 °C

2.1: water; potassium hydroxide / methanol / Reflux

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

4.1: chloro(meso-tetrakis(2,6-dichlorophenyl)porphyrinato)manganese(III); dihydrogen peroxide; sodium hydrogencarbonate / tetrahydrofuran; water / 0.25 h / 20 °C / pH 6.3 / aq. phosphate buffer

With dmap; chloro(meso-tetrakis(2,6-dichlorophenyl)porphyrinato)manganese(III); water; dihydrogen peroxide; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1021/ja208009r

Reference yield:

: 2468-56-6
1-iodo-5-hexyne

: 1356409-37-4
C₄₀H₅₇N₉O₈

: 1356409-90-9
C₄₀H₅₇N₉O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 1.5 h / -78 - 0 °C

2.1: water; potassium hydroxide / methanol / Reflux

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

4.1: chloro(meso-tetrakis(2,6-dichlorophenyl)porphyrinato)manganese(III); dihydrogen peroxide; sodium hydrogencarbonate / tetrahydrofuran; water / 0.25 h / 20 °C / pH 6.3 / aq. phosphate buffer

With dmap; chloro(meso-tetrakis(2,6-dichlorophenyl)porphyrinato)manganese(III); water; dihydrogen peroxide; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1021/ja208009r