C₄₄H₇₀N₂O₁₃

Base Information

Chemical Name:C₄₄H₇₀N₂O₁₃
CAS No.:1332746-56-1
Molecular Formula:C₄₄H₇₀N₂O₁₃
Molecular Weight:835.045
Hs Code.:

C<sub>44</sub>H<sub>70</sub>N<sub>2</sub>O<sub>13</sub>

Synonyms:

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Chemical Property of C₄₄H₇₀N₂O₁₃

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Technology Process of C₄₄H₇₀N₂O₁₃

There total 7 articles about C₄₄H₇₀N₂O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₄₆N₂O₁₁

: 7170-44-7
11-Phenoxyundecanoic acid

: 1332746-56-1
C₄₄H₇₀N₂O₁₃

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c0ob00990c

Reference yield:

: C₅₉H₆₃NO₁₄

: 1332746-56-1
C₄₄H₇₀N₂O₁₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluoroacetic acid / dichloromethane / Inert atmosphere

2.1: pyridine; dmap / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-methylaniline / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.1: piperidine / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

With piperidine; 4-methyl-morpholine; pyridine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-methylaniline; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c0ob00990c

Reference yield:

: C₂₇H₃₁NO₁₀

: 1332746-56-1
C₄₄H₇₀N₂O₁₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine; dmap / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-methylaniline / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

4.1: piperidine / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

With piperidine; 4-methyl-morpholine; pyridine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-methylaniline; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c0ob00990c