C₅₆H₆₃BF₂N₆O₁₆S₄

Base Information

Chemical Name:C₅₆H₆₃BF₂N₆O₁₆S₄
CAS No.:1391916-71-4
Molecular Formula:C₅₆H₆₃BF₂N₆O₁₆S₄
Molecular Weight:1253.22
Hs Code.:

C<sub>56</sub>H<sub>63</sub>BF<sub>2</sub>N<sub>6</sub>O<sub>16</sub>S<sub>4</sub>

Synonyms:

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Chemical Property of C₅₆H₆₃BF₂N₆O₁₆S₄

Chemical Property:

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Technology Process of C₅₆H₆₃BF₂N₆O₁₆S₄

There total 6 articles about C₅₆H₆₃BF₂N₆O₁₆S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1005412-02-1
α-sulfo-β-alaninyl-α-sulfo-β-alanine

: 1391916-79-2
C₅₄H₅₆BF₂N₅O₁₀S₂

: 1391916-71-4
C₅₆H₆₃BF₂N₆O₁₆S₄

Guidance literature:: With sodium hydrogencarbonate; In 1-methyl-pyrrolidin-2-one; water; at 4 - 20 ℃; pH=8.2; Inert atmosphere;
DOI:10.1002/chem.201103613

Reference yield:

: 860003-14-1
4-[3-(dimethylamino)-1-propyn-1-yl]benzaldehyde

: 1391916-71-4
C₅₆H₆₃BF₂N₆O₁₆S₄

Guidance literature:: Multi-step reaction with 6 steps

1: piperidine / toluene / 2 h / 140 °C / Inert atmosphere

2: bis-triphenylphosphine-palladium(II) chloride; triethylamine / 4 h / 60 °C / Inert atmosphere

3: N,N-dimethyl-formamide / 60 °C / Inert atmosphere

4: water; sodium hydroxide / ethanol / 20 °C / Inert atmosphere

5: N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 20 °C / Inert atmosphere

6: sodium hydrogencarbonate / 1-methyl-pyrrolidin-2-one; water / 4 - 20 °C / pH 8.2 / Inert atmosphere

With piperidine; bis-triphenylphosphine-palladium(II) chloride; water; sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In 1-methyl-pyrrolidin-2-one; ethanol; water; N,N-dimethyl-formamide; toluene; 1: Knoevenagel condensation;
DOI:10.1002/chem.201103613

Reference yield:

: 1263506-67-7
[(C(C₄HN(CH₃)CHCHC₆H₄C₂CH₂N(CH₃)2)2C₆H₄I)BF₂]

: 1391916-71-4
C₅₆H₆₃BF₂N₆O₁₆S₄

Guidance literature:: Multi-step reaction with 5 steps

1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / 4 h / 60 °C / Inert atmosphere

2: N,N-dimethyl-formamide / 60 °C / Inert atmosphere

3: water; sodium hydroxide / ethanol / 20 °C / Inert atmosphere

4: N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 20 °C / Inert atmosphere

5: sodium hydrogencarbonate / 1-methyl-pyrrolidin-2-one; water / 4 - 20 °C / pH 8.2 / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; water; sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In 1-methyl-pyrrolidin-2-one; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201103613