C₁₇H₂₆ClIO₃Si

Base Information

Chemical Name:C₁₇H₂₆ClIO₃Si
CAS No.:1622094-22-7
Molecular Formula:C₁₇H₂₆ClIO₃Si
Molecular Weight:468.835
Hs Code.:

C<sub>17</sub>H<sub>26</sub>ClIO<sub>3</sub>Si

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₂₆ClIO₃Si

Chemical Property:

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Technology Process of C₁₇H₂₆ClIO₃Si

There total 5 articles about C₁₇H₂₆ClIO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1622094-35-2
C₁₇H₂₇IO₄Si

: 1622094-22-7
C₁₇H₂₆ClIO₃Si

Guidance literature:: With thionyl chloride; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201402323

Reference yield:

: 179260-96-9
4-methoxy-3-(triisopropylsilyloxy)-benzaldehyde

: 1622094-22-7
C₁₇H₂₆ClIO₃Si

Guidance literature:: Multi-step reaction with 3 steps

1: silver nitrate; iodine / dichloromethane / 14 h / 20 °C / Inert atmosphere

2: copper dichloride; tert.-butylhydroperoxide / acetonitrile; water / 16 h / 20 - 50 °C

3: thionyl chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere; Reflux

With tert.-butylhydroperoxide; thionyl chloride; iodine; silver nitrate; copper dichloride; In dichloromethane; water; acetonitrile;
DOI:10.1002/chem.201402323

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 1622094-22-7
C₁₇H₂₆ClIO₃Si

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

2: silver nitrate; iodine / dichloromethane / 14 h / 20 °C / Inert atmosphere

3: copper dichloride; tert.-butylhydroperoxide / acetonitrile; water / 16 h / 20 - 50 °C

4: thionyl chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere; Reflux

With 1H-imidazole; tert.-butylhydroperoxide; thionyl chloride; iodine; silver nitrate; copper dichloride; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201402323