(μ-SCH2CH2PPh2)2Fe2(CO)4

Base Information

Chemical Name:(μ-SCH2CH2PPh2)2Fe2(CO)4
CAS No.:406185-54-4
Molecular Formula:C₃₂H₂₈Fe₂O₄P₂S₂
Molecular Weight:714.345
Hs Code.:

Synonyms:

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Chemical Property of (μ-SCH2CH2PPh2)2Fe2(CO)4

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Technology Process of (μ-SCH2CH2PPh2)2Fe2(CO)4

There total 2 articles about (μ-SCH2CH2PPh2)2Fe2(CO)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [(μ-H)(anti-(μ-SCH2CH2PPh2)2Fe2(CO)4)][CF3SO3]

: [(μ-H)(syn-(μ-SCH2CH2PPh2)2Fe2(CO)4)][CF3SO3]

: 406185-54-4,405883-69-4
(μ-SCH2CH2PPh2)2Fe2(CO)4

Guidance literature:: With cobaltocene; In acetonitrile; to soln. of Fe-complexes in MeCN was added Cp2Co in MeCN, stirred overnight; monitored by IR;
DOI:10.1021/ic010741g

Reference yield:

: 405883-64-9
Fe(CO)4(P(C₆H₅)2CH₂CH₂SH)

: 406185-54-4,405883-69-4
(μ-SCH2CH2PPh2)2Fe2(CO)4

Guidance literature:: In tetrahydrofuran; byproducts: CO; Irradiation (UV/VIS); Fe-complex in THF was irradiated at 22°C with 450 W Hg lamp for 2h under Ar; solvent was removed under vac., washed with hexane, dried in vacuo, extd. with ether, solvent was removed, dissolved in THF, hexane was added, mother liquor was removed, dried under vac.; elem. anal.;
DOI:10.1021/ic010741g

Reference yield: 65.0%

: 406185-54-4,405883-69-4
(μ-SCH2CH2PPh2)2Fe2(CO)4

: 1493-13-6
trifluorormethanesulfonic acid

: [(μ-H)(anti-(μ-SCH2CH2PPh2)2Fe2(CO)4)][CF3SO3]

Guidance literature:: In tetrahydrofuran; ligand was added to soln. of Fe-complex in THF at room temp. under Ar, stirred for 2 h; solvent was removed, washed with Et2O, extd. with THF, filtered, solventwas removed, Et2O was added; elem. anal.;
DOI:10.1021/ic010741g