{Rh2(μ-N2C(CO2C2H5)2)(CO)2(bis(diphenylphosphino)methane)2}

Base Information

Chemical Name:{Rh2(μ-N2C(CO2C2H5)2)(CO)2(bis(diphenylphosphino)methane)2}
CAS No.:91759-42-1
Molecular Formula:C₅₉H₅₄N₂O₆P₄Rh₂
Molecular Weight:1216.79
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {Rh2(μ-N2C(CO2C2H5)2)(CO)2(bis(diphenylphosphino)methane)2}

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Technology Process of {Rh2(μ-N2C(CO2C2H5)2)(CO)2(bis(diphenylphosphino)methane)2}

There total 2 articles about {Rh2(μ-N2C(CO2C2H5)2)(CO)2(bis(diphenylphosphino)methane)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 5256-74-6
1,3-diethyl 2-diazopropanedioate

: Rh₂H₂(CO)2(bis(phenylphosphino)methane)2

: 91759-42-1
{Rh2(μ-N2C(CO2C2H5)2)(CO)2(bis(diphenylphosphino)methane)2}

Guidance literature:: In tetrahydrofuran; byproducts: H2; Rh2H2(CO)2(dppm)2 was partially dissolved in THF under H2, diethyl diazomalonate was added by syringe to the react. soln., stirred at room temp. for 2-3 h, the product was pptd. with ether and filtered under N2; washed with ether and dried in vac.; elem. anal.;